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High quality TrifluoroMethyl trifluoroMethanesulfonate supplier in China
Cas No: 3582-05-6
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High quality TrifluoroMethyl trifluoroMethanesulfonate supplier in China
Cas No: 3582-05-6
USD $ 1.0-3.0 / Metric Ton 1 Metric Ton 10 Metric Ton/Day Hebei yanxi chemical co.,LTD. Contact Supplier
1,1,1-Trifluoromethanesulfonic acid trifluoromethyl ester
Cas No: 3582-05-6
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(Trifluoromethyl) trifluoromethanesulfonate
Cas No: 3582-05-6
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Trifluoromethyl Trifluoromethanesulfonate_
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BLOOM TECH Advanced API/Technology support TRIFLUOROMETHANESULFONIC ACID TRIFLUOROMETHYL ESTER CAS 3582-05-6
Cas No: 3582-05-6
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High Purity 1,1,1-Trifluoromethanesulfonic acid trifluoromethyl ester Cas No: 3582-05-6
Cas No: 3582-05-6
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Trifluoromethyltrifluoromethanesulfonate
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Methanesulfonicacid, 1,1,1-trifluoro-, trifluoromethyl ester
Cas No: 3582-05-6
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3582-05-6 Usage

Chemical Properties

Colorless to pale yellow liquid
InChI:InChI=1/C2F6O3S/c3-1(4,5)11-12(9,10)2(6,7)8

3582-05-6SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 13, 2017

Revision Date: Aug 13, 2017

1.Identification

1.1 GHS Product identifier

Product name trifluoromethyl trifluoromethanesulfonate

1.2 Other means of identification

Product number -
Other names trifluoromethanesulfonic acid trifluoromethylester

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:3582-05-6 SDS

3582-05-6Synthetic route

trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
With pentafluoroethanesulfonic acid anhydride at 60℃; for 4h;100%
With phosphorus pentoxide In neat (no solvent) at 80 - 180℃; Inert atmosphere;66%
With phosphorus pentoxide at -78 - 110℃; Inert atmosphere;56%
trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
With trifluorormethanesulfonic acid at 180℃; for 24h; Product distribution; other temperatures and different anhydride/acid ratios;100%
With trifluorormethanesulfonic acid at 180℃; for 24h;100%
With trifluorormethanesulfonic acid at 80℃; for 3.3h;97%
Stage #1: trifluoromethylsulfonic anhydride With antimony pentafluoride at -78 - 60℃;
Stage #2: With potassium hydroxide at 15℃;
84%
With antimony pentafluoride
silver trifluoromethanesulfonate
2923-28-6

silver trifluoromethanesulfonate

methyl iodide
74-88-4

methyl iodide

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
In benzene 200°C, 24 h;86%
In benzene 200°C, 24 h;86%
polytetrafluoroethylene
116-14-3

polytetrafluoroethylene

Bromine(I) trifluoromethanesulfonate
70142-16-4

Bromine(I) trifluoromethanesulfonate

A

Bromotrifluoromethane
75-63-8

Bromotrifluoromethane

B

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

C

Trifluoro-methanesulfonic acid 2-bromo-1,1,2,2-tetrafluoro-ethyl ester
73323-42-9

Trifluoro-methanesulfonic acid 2-bromo-1,1,2,2-tetrafluoro-ethyl ester

Conditions
ConditionsYield
at -111 - -55℃; for 10h;A n/a
B n/a
C 83%
perfluoropropylene
116-15-4

perfluoropropylene

Bromine(I) trifluoromethanesulfonate
70142-16-4

Bromine(I) trifluoromethanesulfonate

A

1,2-dibromohexafluoropropane
661-95-0

1,2-dibromohexafluoropropane

B

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

C

Trifluoro-methanesulfonic acid 2-bromo-1,1,2,3,3,3-hexafluoro-propyl ester
73323-45-2

Trifluoro-methanesulfonic acid 2-bromo-1,1,2,3,3,3-hexafluoro-propyl ester

Conditions
ConditionsYield
at -111 - -5℃; for 24h;A n/a
B n/a
C 80%
trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

A

carbon tetrafluoride
75-73-0

carbon tetrafluoride

B

Trifluoromethanesulfonyl fluoride
335-05-7

Trifluoromethanesulfonyl fluoride

C

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
With antimony pentafluoride at 25 - 60℃; for 0.25h; Yields of byproduct given;A n/a
B n/a
C 80%
With antimony pentafluoride at 25 - 60℃; for 0.25h; Product distribution; Mechanism; var. Lewis acids, time, and temp.;A n/a
B n/a
C 87 % Spectr.
2-(trifluoromethoxy)biphenylyl-2'-diazonium triflate

2-(trifluoromethoxy)biphenylyl-2'-diazonium triflate

A

2-(trifluoromethanesulfonyloxy)-2'-(trifluoromethoxy)biphenyl

2-(trifluoromethanesulfonyloxy)-2'-(trifluoromethoxy)biphenyl

B

dibenzofuran
132-64-9

dibenzofuran

C

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
In dichloromethane-d2 at 42℃; for 3h;A 14%
B 75%
C n/a
perfluoroethanesulfonic acid
354-88-1

perfluoroethanesulfonic acid

trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

A

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

B

pentafluoroethanesulfonate de trifluoromethyle
77927-85-6

pentafluoroethanesulfonate de trifluoromethyle

Conditions
ConditionsYield
at 120℃; for 10h; Product distribution; other reaction temperatures and times; different anhydride/acid ratios;A 54%
B 46 % Spectr.
at 80℃; for 15h; Title compound not separated from byproducts;A 25%
B 75 % Spectr.
at 80℃; for 15h; other acid and anhydride ratio, other temperature and time;
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

pentafluoroethanesulfonic acid anhydride
51604-58-1

pentafluoroethanesulfonic acid anhydride

A

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

B

pentafluoroethanesulfonate de trifluoromethyle
77927-85-6

pentafluoroethanesulfonate de trifluoromethyle

C

pentafluoroethyl pentafluoroethanesulfonate
77927-84-5

pentafluoroethyl pentafluoroethanesulfonate

Conditions
ConditionsYield
at 100℃; for 6h; Product distribution; other reaction temperatures and times; different anhydride/acid ratios;A 44%
B 44 % Spectr.
C 12%
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
reflux;19%
reflux;19%
Bromine(I) trifluoromethanesulfonate
70142-16-4

Bromine(I) trifluoromethanesulfonate

A

Dichlorodifluoromethane
75-71-8

Dichlorodifluoromethane

B

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

C

perfluorochloromethyl trifluoromethanesulfonate
74501-96-5

perfluorochloromethyl trifluoromethanesulfonate

D

difluoromethyl bis(trifluoromethanesulfonate)
74512-41-7

difluoromethyl bis(trifluoromethanesulfonate)

Conditions
ConditionsYield
at -111 - -50℃; for 15h; Further byproducts given;A 0.6 mmol
B 0.7 mmol
C 0.6 mmol
D 0.12 mmol
Dichlorodifluoromethane
75-71-8

Dichlorodifluoromethane

Bromine(I) trifluoromethanesulfonate
70142-16-4

Bromine(I) trifluoromethanesulfonate

A

trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

B

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

C

perfluorochloromethyl trifluoromethanesulfonate
74501-96-5

perfluorochloromethyl trifluoromethanesulfonate

D

difluoromethyl bis(trifluoromethanesulfonate)
74512-41-7

difluoromethyl bis(trifluoromethanesulfonate)

Conditions
ConditionsYield
at -111 - -50℃; for 15h; Further byproducts given;A 0.6 mmol
B 0.7 mmol
C 0.6 mmol
D 0.12 mmol
trichlorofluoromethane
75-69-4

trichlorofluoromethane

Bromine(I) trifluoromethanesulfonate
70142-16-4

Bromine(I) trifluoromethanesulfonate

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
at -111 - -10℃; for 15h;2.9 mmol
Bromotrifluoromethane
75-63-8

Bromotrifluoromethane

Chlorine(I) trifluoromethanesulfonate
65597-24-2

Chlorine(I) trifluoromethanesulfonate

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
at -111℃; for 1h;3.8 mmol
at -111℃; for 1h; Product distribution; reactions of chlorine(I) and bromine(I) trifluoromethanesulfonates with various perfluoroalkyl halides;3.8 mmol
dibromodifluoromethane
75-61-6

dibromodifluoromethane

Bromine(I) trifluoromethanesulfonate
70142-16-4

Bromine(I) trifluoromethanesulfonate

A

trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

B

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

C

perfluorobromomethyl trifluoromethanesulfonate
74501-92-1

perfluorobromomethyl trifluoromethanesulfonate

D

difluoromethyl bis(trifluoromethanesulfonate)
74512-41-7

difluoromethyl bis(trifluoromethanesulfonate)

Conditions
ConditionsYield
at -111 - -60℃; for 24h; Further byproducts given;A 0.35 mmol
B 0.4 mmol
C 0.7 mmol
D 0.7 mmol
1,2-dibromo-1,1,2,2-tetrafluoroethane
124-73-2

1,2-dibromo-1,1,2,2-tetrafluoroethane

Chlorine(I) trifluoromethanesulfonate
65597-24-2

Chlorine(I) trifluoromethanesulfonate

A

bromopentafluoroethane
354-55-2

bromopentafluoroethane

B

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

C

Trifluoro-methanesulfonic acid 2-bromo-1,1,2,2-tetrafluoro-ethyl ester
73323-42-9

Trifluoro-methanesulfonic acid 2-bromo-1,1,2,2-tetrafluoro-ethyl ester

Conditions
ConditionsYield
at -111 - -88℃; for 1h;A 0.4 mmol
B 0.8 mmol
C 1.7 mmol
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

pentafluoroethanesulfonate de trifluoromethyle
77927-85-6

pentafluoroethanesulfonate de trifluoromethyle

A

perfluoroethanesulfonic acid
354-88-1

perfluoroethanesulfonic acid

B

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

C

pentafluoroethyl pentafluoroethanesulfonate
77927-84-5

pentafluoroethyl pentafluoroethanesulfonate

Conditions
ConditionsYield
at 190℃; for 40h; Product distribution;
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

pentafluoroethyl pentafluoroethanesulfonate
77927-84-5

pentafluoroethyl pentafluoroethanesulfonate

A

perfluoroethanesulfonic acid
354-88-1

perfluoroethanesulfonic acid

B

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

C

trifluoroacetic acid
76-05-1

trifluoroacetic acid

Conditions
ConditionsYield
at 190℃; for 90h; Product distribution; other perfluoroalkane sulfonic acid;
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

pentafluoroethanesulfonic acid anhydride
51604-58-1

pentafluoroethanesulfonic acid anhydride

A

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

B

pentafluoroethanesulfonate de trifluoromethyle
77927-85-6

pentafluoroethanesulfonate de trifluoromethyle

Conditions
ConditionsYield
at 80℃; for 6h; other acid and anhydride ratio, other temperature and time;
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

pentafluoroethyl pentafluoroethanepyrosulfonate de perfluoroethyle

pentafluoroethyl pentafluoroethanepyrosulfonate de perfluoroethyle

A

trifluoroacetyl fluoride
354-34-7

trifluoroacetyl fluoride

B

perfluoroethanesulfonic acid
354-88-1

perfluoroethanesulfonic acid

C

trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

D

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
at 45℃; for 14h; Product distribution;
tris(trifluoromethanesulfonyloxy)boron
64371-01-3

tris(trifluoromethanesulfonyloxy)boron

A

Carbonyl fluoride
353-50-4

Carbonyl fluoride

B

trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

C

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
In neat (no solvent) at 200℃; for 1h;
Bromine(I) trifluoromethanesulfonate
70142-16-4

Bromine(I) trifluoromethanesulfonate

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
With chlorotrifluorosilane at -130 - -22℃;
thermal decompn. at 22°C;
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

A

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

B

SO2, H3PO4

SO2, H3PO4

Conditions
ConditionsYield
With phosphorus pentoxide other reagent;
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

A

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

B

SO2

SO2

Conditions
ConditionsYield
at 180℃; for 1h; other perfluoroalkanesulfonic anhydrides and corresponding acids, thermal stability;
at 180℃; for 1h;
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
at 176.84℃;
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

A

Trifluoromethanesulfonyl fluoride
335-05-7

Trifluoromethanesulfonyl fluoride

B

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

A

Carbonyl fluoride
353-50-4

Carbonyl fluoride

B

Hexafluoroethane
76-16-4

Hexafluoroethane

C

trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

D

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
byproducts: SO3, SOF2; at 10°C;
bis(trifluoromethanesulfonyl)peroxide
4079-87-2

bis(trifluoromethanesulfonyl)peroxide

A

Hexafluoroethane
76-16-4

Hexafluoroethane

B

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

C

sulfur trioxide
7446-11-9

sulfur trioxide

Conditions
ConditionsYield
10°C;
Dichlorodifluoromethane
75-71-8

Dichlorodifluoromethane

Bromine(I) trifluoromethanesulfonate
70142-16-4

Bromine(I) trifluoromethanesulfonate

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Conditions
ConditionsYield
in 2 : 1 mixture, -111- -50°C, 15 h;
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

2-amino-4-methoxyphenol
20734-76-3

2-amino-4-methoxyphenol

5-methoxy-3H-benzooxazol-2-one
40925-63-1

5-methoxy-3H-benzooxazol-2-one

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;99%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

3'-Amino-2'-hydroxyacetophenone
70977-72-9

3'-Amino-2'-hydroxyacetophenone

7-acetylbenzo[d]oxazol-2(3H)-one

7-acetylbenzo[d]oxazol-2(3H)-one

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;99%
2-Aminobenzyl alcohol
5344-90-1

2-Aminobenzyl alcohol

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

1,4-dihydro-2H-benzo[d][1,3]oxazin-2-one
13213-88-2

1,4-dihydro-2H-benzo[d][1,3]oxazin-2-one

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;99%
morpholine
110-91-8

morpholine

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

morpholine-4-carbonyl fluoride
68928-13-2

morpholine-4-carbonyl fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.0333333h; Sealed tube;99%
C3H9F2Si(1-)*C7H18N3(1+)
478945-43-6, 551925-01-0

C3H9F2Si(1-)*C7H18N3(1+)

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

A

tris(dimethylamino)methylium trifluoromethanolate
1006904-67-1

tris(dimethylamino)methylium trifluoromethanolate

B

Trifluoromethanesulfonyl fluoride
335-05-7

Trifluoromethanesulfonyl fluoride

Conditions
ConditionsYield
In acetonitrile at -30℃;A 98%
B n/a
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

desloratadine

desloratadine

4-(3-chloro-5,6-dihydro-11H-benzo[5,6]cyclohepta[1,2-b]pyridin-11-ylidene)piperidine-1-carbonyl fluoride

4-(3-chloro-5,6-dihydro-11H-benzo[5,6]cyclohepta[1,2-b]pyridin-11-ylidene)piperidine-1-carbonyl fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.0333333h; Sealed tube;98%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

4-tert-Butylaniline
769-92-6

4-tert-Butylaniline

1,3-bis(4-(tert-butyl)phenyl)urea
78015-86-8

1,3-bis(4-(tert-butyl)phenyl)urea

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;98%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

4-Aminoacetophenone
99-92-3

4-Aminoacetophenone

1,3-bis(4-acetylphenyl)urea
20782-48-3

1,3-bis(4-acetylphenyl)urea

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;98%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

8-amino-1-naphthol
2834-91-5

8-amino-1-naphthol

1,3-bis(7-hydroxynaphthalen-1-yl)urea

1,3-bis(7-hydroxynaphthalen-1-yl)urea

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;97%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

3,3α,8,8α-tetrahydro-2H-indeno[1,2-d]oxazol-2-one
114364-45-3

3,3α,8,8α-tetrahydro-2H-indeno[1,2-d]oxazol-2-one

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;97%
3-cyclohexylaminopropionitrile
702-03-4

3-cyclohexylaminopropionitrile

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

(2-cyanoethyl)(cyclohexyl)carbamic fluoride

(2-cyanoethyl)(cyclohexyl)carbamic fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.0333333h; Sealed tube;97%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

amoxapine
14028-44-5

amoxapine

4-(2-chlorodibenzo[b,f][1,4]oxazepin-11-yl)piperazine-1-carbonyl fluoride

4-(2-chlorodibenzo[b,f][1,4]oxazepin-11-yl)piperazine-1-carbonyl fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.0833333h; Sealed tube;97%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

troxipide
30751-05-4

troxipide

3-(3,4,5-trimethoxybenzamido)piperidine-1-carbonyl fluoride

3-(3,4,5-trimethoxybenzamido)piperidine-1-carbonyl fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.0833333h; Sealed tube;97%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

dibenzylamine
103-49-1

dibenzylamine

N,N-dibenzylcarbamoyl fluoride

N,N-dibenzylcarbamoyl fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.0333333h; Solvent; Sealed tube;96%
In acetonitrile at 20℃; for 0.166667h; Sealed tube; Large scale;91%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Riluzole
1744-22-5

Riluzole

1,3-bis(6-(trifluoromethoxy)benzo[d]thiazol-2-yl)urea

1,3-bis(6-(trifluoromethoxy)benzo[d]thiazol-2-yl)urea

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;96%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

p-toluidine
106-49-0

p-toluidine

1,3-di-p-tolylurea
621-00-1

1,3-di-p-tolylurea

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;96%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

4-fluoroaniline
371-40-4

4-fluoroaniline

N,N'-Di-(4-Fluorphenyl)-harnstoff
370-22-9

N,N'-Di-(4-Fluorphenyl)-harnstoff

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;96%
Thiomorpholin
123-90-0

Thiomorpholin

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

thiomorpholine-4-carbonyl fluoride

thiomorpholine-4-carbonyl fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.0833333h; Sealed tube;95%
In acetonitrile at 20℃; for 0.0333333h; Sealed tube;95%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

N-cyclohexyl-cyclohexanamine
101-83-7

N-cyclohexyl-cyclohexanamine

dicyclohexylcarbamic fluoride

dicyclohexylcarbamic fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.0333333h; Sealed tube;95%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

4-Aminobiphenyl
92-67-1

4-Aminobiphenyl

1,3-di([1,1'-biphenyl]-4-yl)urea
95745-38-3

1,3-di([1,1'-biphenyl]-4-yl)urea

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;95%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

ethyl (E)-2-diazooct-3-enoate

ethyl (E)-2-diazooct-3-enoate

ethyl (E)-4-(trifluoromethoxy)oct-2-enoate

ethyl (E)-4-(trifluoromethoxy)oct-2-enoate

Conditions
ConditionsYield
With silver fluoride In acetonitrile at -30 - 10℃; Inert atmosphere;94%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

ethyl 2-diazo-3-octenoate

ethyl 2-diazo-3-octenoate

ethyl 4-trifluoromethoxy-2-octenoate

ethyl 4-trifluoromethoxy-2-octenoate

Conditions
ConditionsYield
With silver fluoride In acetonitrile at -30 - 10℃; Inert atmosphere;94%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

phenethylamine
64-04-0

phenethylamine

1,3-diphenethylurea
5467-84-5

1,3-diphenethylurea

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;94%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

3,4-methylenedioxyphenylethylamine
1484-85-1

3,4-methylenedioxyphenylethylamine

1,3-bis(2-(benzo[d][1,3]dioxol-5-yl)ethyl)urea

1,3-bis(2-(benzo[d][1,3]dioxol-5-yl)ethyl)urea

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.25h; Sealed tube;94%
1-(2-chloro-6-fluorobenzyl)piperazine

1-(2-chloro-6-fluorobenzyl)piperazine

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

4-(2-chloro-6-fluorobenzyl)piperazine-1-carbonyl fluoride

4-(2-chloro-6-fluorobenzyl)piperazine-1-carbonyl fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.0333333h; Sealed tube;94%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

Adofen
56296-78-7

Adofen

N-methyl-N-{3-phenyl-3-[4-(trifluoromethyl)phenoxy]propyl}carbamoyl fluoride

N-methyl-N-{3-phenyl-3-[4-(trifluoromethyl)phenoxy]propyl}carbamoyl fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.0333333h; Sealed tube;94%
phenylethane 1,2-diol
93-56-1

phenylethane 1,2-diol

trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

4-Phenyl-1,3-dioxolan-2-one
4427-92-3

4-Phenyl-1,3-dioxolan-2-one

Conditions
ConditionsYield
With triethylamine In acetonitrile at 20℃; for 1h; Reagent/catalyst; Sealed tube;94%
trifluoromethyl trifluoromethanesulfonate
3582-05-6

trifluoromethyl trifluoromethanesulfonate

benzylamine
100-46-9

benzylamine

1,3-dibenzylurea
1466-67-7

1,3-dibenzylurea

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Sealed tube;93%

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