C₃₁H₂₈N₃O₃P

Base Information Edit

Chemical Name:C₃₁H₂₈N₃O₃P
CAS No.:290333-05-0
Molecular Formula:C₃₁H₂₈N₃O₃P
Molecular Weight:521.555
Hs Code.:
Mol file:290333-05-0.mol

C<sub>31</sub>H<sub>28</sub>N<sub>3</sub>O<sub>3</sub>P

Synonyms:C₃₁H₂₈N₃O₃P

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Chemical Property of C₃₁H₂₈N₃O₃P Edit

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Technology Process of C₃₁H₂₈N₃O₃P

There total 10 articles about C₃₁H₂₈N₃O₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 290333-04-9
C₃₇H₄₂N₃O₄PSi

: 290333-05-0
C₃₁H₂₈N₃O₃P

Guidance literature:: With tetrabutyl ammonium fluoride; silica gel; In tetrahydrofuran; for 0.0166667h; microwave heating;
DOI:10.1016/S0040-4039(00)00728-0

Reference yield:

: 290332-96-6
ethyl α-azido-β-(4-methoxypyrid-3-yl)acrylate

: 290333-05-0
C₃₁H₂₈N₃O₃P

Guidance literature:: Multi-step reaction with 7 steps

1: 67 percent / o-xylene / 0.42 h / 170 °C

2: 94 percent / sodium hydride / dimethylformamide / 12 h / 20 °C

3: 93 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

4: 86 percent / MnO₂ / CH₂Cl₂ / 72 h / 20 °C

5: 85 percent / Na / ethanol / 72 h / -15 °C

6: 82 percent / CH₂Cl₂ / 24 h / 20 °C

7: 70 percent / Bu₄NF/SiO₂ / 0.03 h / microwave irradiation

With manganese(IV) oxide; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; sodium; silica gel; sodium hydride; In tetrahydrofuran; ethanol; dichloromethane; o-xylene; N,N-dimethyl-formamide; 6: Staudinger reaction;
DOI:10.1021/jo026508x

Reference yield:

: 290332-97-7
2-ethoxycarbonyl-4-methoxypyrrolo[2,3-b]pyridine

: 290333-05-0
C₃₁H₂₈N₃O₃P

Guidance literature:: Multi-step reaction with 6 steps

1.1: 94 percent / sodium hydride / dimethylformamide / 12 h / 20 °C

2.1: 93 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

3.1: 86 percent / MnO₂ / CH₂Cl₂ / 72 h / 20 °C

4.1: 85 percent / Na / ethanol / 72 h / -15 °C

5.1: BF₃*OEt₂ / CH₂Cl₂ / 3 h / 20 °C

5.2: NaOH / CH₂Cl₂; H₂O / 3 h

6.1: 1.59 g / CH₂Cl₂ / 12 h / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; sodium; sodium hydride; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 6.1: Staudinger reaction;
DOI:10.1021/jo026508x