N₃-(2-methoxy-5-morpholin-4-yl-phenyl)-1-pyridin-2-yl-1H-[1,2,4]triazoIe-3,5-diamine

Base Information

• Chemical Name: N₃-(2-methoxy-5-morpholin-4-yl-phenyl)-1-pyridin-2-yl-1H-[1,2,4]triazoIe-3,5-diamine
• CAS No.: 700809-92-3
• Molecular Formula: C₁₈H₂₁N₇O₂
• Molecular Weight: 367.41

Synonyms:N₃-(2-methoxy-5-morpholin-4-yl-phenyl)-1-pyridin-2-yl-1H-[1,2,4]triazoIe-3,5-diamine

Chemical Property of N₃-(2-methoxy-5-morpholin-4-yl-phenyl)-1-pyridin-2-yl-1H-[1,2,4]triazoIe-3,5-diamine

Chemical Property:

Purity/Quality:

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Technology Process of N₃-(2-methoxy-5-morpholin-4-yl-phenyl)-1-pyridin-2-yl-1H-[1,2,4]triazoIe-3,5-diamine

There total 3 articles about N₃-(2-methoxy-5-morpholin-4-yl-phenyl)-1-pyridin-2-yl-1H-[1,2,4]triazoIe-3,5-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1'-oxybis(2-bromo-ethane) (5414-19-7) + N3-(5-amino-2-methoxy-phenyl)-1-pyridin-2-yl-1H-[1,2,4]triazole-3,5-diamine → N3-(2-methoxy-5-morpholin-4-yl-phenyl)-1-pyridin-2-yl-1H-[1,2,4]triazoIe-3,5-diamine (700809-92-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In toluene; at 110 ℃; for 70h;

Reference yield:

2-methoxy-5-morpholin-4-ylaniline (383870-88-0) → N3-(2-methoxy-5-morpholin-4-yl-phenyl)-1-pyridin-2-yl-1H-[1,2,4]triazoIe-3,5-diamine (700809-92-3)

Guidance literature:

Multi-step reaction with 2 steps

1: isopropyl alcohol / 100 °C

2: Heating

In isopropyl alcohol;

DOI:10.1021/jm200712h

Reference yield:

pyrid-2-ylhydrazine (4930-98-7) + C19H20N4O3 → N3-(2-methoxy-5-morpholin-4-yl-phenyl)-1-pyridin-2-yl-1H-[1,2,4]triazoIe-3,5-diamine (700809-92-3)

Guidance literature:

Heating;

DOI:10.1021/jm200712h

upstream raw materials:

1,1'-oxybis(2-bromo-ethane)

pyrid-2-ylhydrazine

2-methoxy-5-morpholin-4-ylaniline

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