3-{benzyl-[1-(1-{[benzyl-(3-hydroxy-propyl)-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-amino}-propan-1-ol

Base Information

Chemical Name:3-{benzyl-[1-(1-{[benzyl-(3-hydroxy-propyl)-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-amino}-propan-1-ol
CAS No.:306776-48-7
Molecular Formula:C₃₄H₅₂N₂O₂S₂
Molecular Weight:584.931
Hs Code.:

Synonyms:3-{benzyl-[1-(1-{[benzyl-(3-hydroxy-propyl)-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-amino}-propan-1-ol

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Chemical Property of 3-{benzyl-[1-(1-{[benzyl-(3-hydroxy-propyl)-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-amino}-propan-1-ol

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Technology Process of 3-{benzyl-[1-(1-{[benzyl-(3-hydroxy-propyl)-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-amino}-propan-1-ol

There total 4 articles about 3-{benzyl-[1-(1-{[benzyl-(3-hydroxy-propyl)-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-amino}-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.6%

: 100-39-0
benzyl bromide

: 306776-70-5
3-[({[({[(3-Hydroxypropyl)amino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)amino]propan-1-ol

: 306776-48-7
3-{benzyl-[1-(1-{[benzyl-(3-hydroxy-propyl)-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-amino}-propan-1-ol

Guidance literature:: With potassium carbonate; In acetone; at 60 ℃; for 12h;
DOI:10.1021/jm000178w

Reference yield:

: 52958-74-4
1-[(2-formylcyclohexyl)disulfanyl]cyclohexanecarbaldehyde

: 306776-48-7
3-{benzyl-[1-(1-{[benzyl-(3-hydroxy-propyl)-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-amino}-propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: MgSO₄ / CHCl₃ / 8 h / Heating

2: NaBH₄ / methanol / 1 h / 20 °C

3: 91.6 percent / K₂CO₃ / acetone / 12 h / 60 °C

With sodium tetrahydroborate; magnesium sulfate; potassium carbonate; In methanol; chloroform; acetone; 1: Condensation / 2: Reduction / 3: Alkylation;
DOI:10.1021/jm000178w

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 306776-48-7
3-{benzyl-[1-(1-{[benzyl-(3-hydroxy-propyl)-amino]-methyl}-cyclohexyldisulfanyl)-cyclohexylmethyl]-amino}-propan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / S₂Cl₂ / various solvent(s) / 2 h / 55 °C

2: MgSO₄ / CHCl₃ / 8 h / Heating

3: NaBH₄ / methanol / 1 h / 20 °C

4: 91.6 percent / K₂CO₃ / acetone / 12 h / 60 °C

With disulfur dichloride; sodium tetrahydroborate; magnesium sulfate; potassium carbonate; In methanol; chloroform; acetone; 1: Dimerization / 2: Condensation / 3: Reduction / 4: Alkylation;
DOI:10.1021/jm000178w