RuCl(C₂C₆H₅)(CO)(P(C(CH₃)3)2CH₃)2

Base Information

Chemical Name:RuCl(C₂C₆H₅)(CO)(P(C(CH₃)3)2CH₃)2
CAS No.:184003-37-0
Molecular Formula:C₂₇H₄₇ClOP₂Ru
Molecular Weight:586.14
Hs Code.:

RuCl(C<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)(CO)(P(C(CH<sub>3</sub>)3)2CH<sub>3</sub>)2

Synonyms:RuCl(C₂C₆H₅)(CO)(P(C(CH₃)3)2CH₃)2

Suppliers and Price of RuCl(C₂C₆H₅)(CO)(P(C(CH₃)3)2CH₃)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of RuCl(C₂C₆H₅)(CO)(P(C(CH₃)3)2CH₃)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of RuCl(C₂C₆H₅)(CO)(P(C(CH₃)3)2CH₃)2

There total 2 articles about RuCl(C₂C₆H₅)(CO)(P(C(CH₃)3)2CH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 183555-82-0,184180-52-7
RuCl₂(CO)(P(C(CH₃)3)2CH₃)2

: 536-74-3
phenylacetylene

: 184003-37-0
RuCl(C₂C₆H₅)(CO)(P(C(CH₃)3)2CH₃)2

Guidance literature:: With Et₃N; In toluene; absence of air and moisture; 1 equiv. alkyne, 3 equiv. Et3N, warming from -40°C to room temp., stirring for 24 h; filtration (Celite), evapn., extn. into pentane, concn., crystn. (-40°C), collection (filtration), washing (pentane), drying (vac.); elem. anal.;
DOI:10.1021/ic9605837

Reference yield:

: 183555-82-0,184180-52-7
RuCl₂(CO)(P(C(CH₃)3)2CH₃)2

: 536-74-3
phenylacetylene

: 184003-37-0
RuCl(C₂C₆H₅)(CO)(P(C(CH₃)3)2CH₃)2

: 184180-53-8,151306-35-3
Ru(C₂C₆H₅)2(CO)(P(C(CH₃)3)2CH₃)2

: 184003-36-9
HP(C(CH₃)3)2CH₃⁽¹⁺⁾*Ru₂Cl₅(CO)2(P(C(CH₃)3)2CH₃)2^(1-)=[HP(C(CH₃)3)2CH₃][Ru₂Cl₅(CO)2(P(C(CH₃)3)2CH₃)2]

Guidance literature:: In benzene; byproducts: MeP(t-Bu)2; absence of air and moisture; 1 equiv. alkyne; not isolated, detd. by NMR spectroscopy;
DOI:10.1021/ic9605837

Reference yield:

: 184003-37-0
RuCl(C₂C₆H₅)(CO)(P(C(CH₃)3)2CH₃)2

: 201230-82-2
carbon monoxide

: 184003-40-5,184180-54-9
trans,cis-RuCl(C₂Ph)(CO)2(P(C(CH₃)3)2CH₃)2

Guidance literature:: In toluene; 1 atm CO, warming from -78°C to room temp.; not isolated, reaction followed by NMR and IR spectroscopy;
DOI:10.1021/ic9605837