2-fluoro-2-deoxy-3-O-acetyl-5-O-(p-nitrobenzoyl)-D-arabinofuranosyl bromide

Base Information

Chemical Name:2-fluoro-2-deoxy-3-O-acetyl-5-O-(p-nitrobenzoyl)-D-arabinofuranosyl bromide
CAS No.:133473-73-1
Molecular Formula:C₁₄H₁₃BrFNO₇
Molecular Weight:406.162
Hs Code.:

Synonyms:2-fluoro-2-deoxy-3-O-acetyl-5-O-(p-nitrobenzoyl)-D-arabinofuranosyl bromide

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Chemical Property of 2-fluoro-2-deoxy-3-O-acetyl-5-O-(p-nitrobenzoyl)-D-arabinofuranosyl bromide

Chemical Property:

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Technology Process of 2-fluoro-2-deoxy-3-O-acetyl-5-O-(p-nitrobenzoyl)-D-arabinofuranosyl bromide

There total 4 articles about 2-fluoro-2-deoxy-3-O-acetyl-5-O-(p-nitrobenzoyl)-D-arabinofuranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₄FNO₈

: 133473-73-1
2-fluoro-2-deoxy-3-O-acetyl-5-O-(p-nitrobenzoyl)-D-arabinofuranosyl bromide

Guidance literature:: With hydrogen bromide; In acetic acid;

Reference yield:

: 4-Nitro-benzoic acid (2R,3R,4S)-3,5-diacetoxy-4-fluoro-tetrahydro-furan-2-ylmethyl ester

: 133473-73-1
2-fluoro-2-deoxy-3-O-acetyl-5-O-(p-nitrobenzoyl)-D-arabinofuranosyl bromide

Guidance literature:: With hydrogen bromide; In dichloromethane; Yield given; Ambient temperature;
DOI:10.1021/jo00011a029

Reference yield:

: 2-fluoro-2-deoxy-5-O-(p-nitrobenzoyl)-D-arabinofuranose

: 133473-73-1
2-fluoro-2-deoxy-3-O-acetyl-5-O-(p-nitrobenzoyl)-D-arabinofuranosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / Ambient temperature

2: aq. HBr / CH₂Cl₂ / Ambient temperature

With pyridine; hydrogen bromide; In dichloromethane;
DOI:10.1021/jo00011a029