3-fluoro-3-deoxy-6-O-(p-nitrobenzoyl)-1,2-O-isopropylidene-α-D-glucofuranose

Base Information

Chemical Name:3-fluoro-3-deoxy-6-O-(p-nitrobenzoyl)-1,2-O-isopropylidene-α-D-glucofuranose
CAS No.:133473-70-8
Molecular Formula:C₁₆H₁₈FNO₈
Molecular Weight:371.319
Hs Code.:

Synonyms:3-fluoro-3-deoxy-6-O-(p-nitrobenzoyl)-1,2-O-isopropylidene-α-D-glucofuranose

Suppliers and Price of 3-fluoro-3-deoxy-6-O-(p-nitrobenzoyl)-1,2-O-isopropylidene-α-D-glucofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-fluoro-3-deoxy-6-O-(p-nitrobenzoyl)-1,2-O-isopropylidene-α-D-glucofuranose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-fluoro-3-deoxy-6-O-(p-nitrobenzoyl)-1,2-O-isopropylidene-α-D-glucofuranose

There total 3 articles about 3-fluoro-3-deoxy-6-O-(p-nitrobenzoyl)-1,2-O-isopropylidene-α-D-glucofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 18530-81-9
(R)-1-((3aR,5R,6S,6aS)-6-fluoro-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethane-1,2-diol

: 122-04-3
4-nitro-benzoyl chloride

: 133473-70-8
3-fluoro-3-deoxy-6-O-(p-nitrobenzoyl)-1,2-O-isopropylidene-α-D-glucofuranose

Guidance literature:: With pyridine; In dichloromethane; at -20 ℃;
DOI:10.1021/jo00011a029

Reference yield:

: 14686-89-6
(1,2:5,6)-di-O-isopropylidene-D-gulose

: 133473-70-8
3-fluoro-3-deoxy-6-O-(p-nitrobenzoyl)-1,2-O-isopropylidene-α-D-glucofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / (diethylamino)sulfur trifluoride

2: 98 percent / aq. H₂SO₄ / dioxane; ethanol / 4 h / Ambient temperature

3: 80 percent / pyridine / CH₂Cl₂ / -20 °C

With pyridine; diethylamino-sulfur trifluoride; sulfuric acid; In 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1021/jo00011a029

Reference yield:

: 14049-05-9
3-deoxy-1,2;5,6-di-O-isopropylidene-3-fluoro-α-D-glucofuranose

: 133473-70-8
3-fluoro-3-deoxy-6-O-(p-nitrobenzoyl)-1,2-O-isopropylidene-α-D-glucofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / aq. H₂SO₄ / dioxane; ethanol / 4 h / Ambient temperature

2: 80 percent / pyridine / CH₂Cl₂ / -20 °C

With pyridine; sulfuric acid; In 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1021/jo00011a029