bis[p-(3-carbomethoxy-5-hydroxyphenoxy)phenyl] sulfone

Base Information

Chemical Name:bis[p-(3-carbomethoxy-5-hydroxyphenoxy)phenyl] sulfone
CAS No.:197242-29-8
Molecular Formula:C₂₈H₂₂O₁₀S
Molecular Weight:550.543
Hs Code.:

Synonyms:bis[p-(3-carbomethoxy-5-hydroxyphenoxy)phenyl] sulfone

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Chemical Property of bis[p-(3-carbomethoxy-5-hydroxyphenoxy)phenyl] sulfone

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Technology Process of bis[p-(3-carbomethoxy-5-hydroxyphenoxy)phenyl] sulfone

There total 4 articles about bis[p-(3-carbomethoxy-5-hydroxyphenoxy)phenyl] sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 197242-32-3
bis[p-[3-(benzyloxy)-5-carbomethoxyphenoxy]phenyl] sulfone

: 197242-29-8
bis[p-(3-carbomethoxy-5-hydroxyphenoxy)phenyl] sulfone

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 0.5h; under 3102.9 Torr;
DOI:10.1021/jo970954g

Reference yield:

: 54915-31-0
methyl 3-(benzyloxy)-5-hydroxybenzoate

: 197242-29-8
bis[p-(3-carbomethoxy-5-hydroxyphenoxy)phenyl] sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) K₂CO₃ / 1) DMAc, toluene, reflux, 25 h; 2) DMAc, 160 deg C, 24 h

2: 88 percent / H₂ / Pd/C / ethyl acetate / 0.5 h / 3102.9 Torr

With hydrogen; potassium carbonate; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/jo970954g

Reference yield:

: 100-39-0
benzyl bromide

: 197242-29-8
bis[p-(3-carbomethoxy-5-hydroxyphenoxy)phenyl] sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1) DMF, 110 deg C, 5 h; 2) DMF, rt, 3 d

2: 1.) K₂CO₃ / 1) DMAc, toluene, reflux, 25 h; 2) DMAc, 160 deg C, 24 h

3: 88 percent / H₂ / Pd/C / ethyl acetate / 0.5 h / 3102.9 Torr

With hydrogen; sodium hydride; potassium carbonate; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/jo970954g