ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate

Base Information

Chemical Name:ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate
CAS No.:844697-15-0
Molecular Formula:C₃₃H₄₄N₂O₅
Molecular Weight:548.723
Hs Code.:

Synonyms:ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate

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Chemical Property of ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate

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Technology Process of ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate

There total 1 articles about ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 3943-89-3
Ethyl protocatechuate

: 5-(6-bromohexyloxy)-2-(4-octylphenyl)pyrimidine

: 844697-15-0
ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate

Guidance literature:: With potassium carbonate; In cyclohexanone; at 70 ℃; for 8h;
DOI:10.1039/b406716a

Reference yield: 57.0%

: 844697-10-5
2-[4-(6-bromohexyloxy)phenyl]-5-octylpyrimidine

: 844697-15-0
ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate

: 844697-16-1
ethyl 3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoate

Guidance literature:: With potassium carbonate; potassium iodide; In cyclohexanone; at 145 ℃; for 10h;
DOI:10.1039/b406716a

Reference yield:

: 844697-15-0
ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate

: 844697-17-2
3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / K₂CO₃; KI / cyclohexanone / 10 h / 145 °C

2: 90 percent / KOH / aq. ethanol / Heating

With potassium hydroxide; potassium carbonate; potassium iodide; In ethanol; cyclohexanone;
DOI:10.1039/b406716a