ethyl 3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoate

Base Information

• Chemical Name: ethyl 3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoate
• CAS No.: 844697-16-1
• Molecular Formula: C₅₇H₇₈N₄O₆
• Molecular Weight: 915.27

Synonyms:ethyl 3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoate

Chemical Property of ethyl 3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoate

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Technology Process of ethyl 3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoate

There total 5 articles about ethyl 3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

2-[4-(6-bromohexyloxy)phenyl]-5-octylpyrimidine (844697-10-5) + ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate (844697-15-0) → ethyl 3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoate (844697-16-1)

Guidance literature:

With potassium carbonate; potassium iodide; In cyclohexanone; at 145 ℃; for 10h;

DOI:10.1039/b406716a

Reference yield:

1 ,6-dibromohexane (629-03-8) → ethyl 3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoate (844697-16-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / K₂CO₃ / cyclohexanone / 6 h / 80 °C

2: 57 percent / K₂CO₃; KI / cyclohexanone / 10 h / 145 °C

With potassium carbonate; potassium iodide; In cyclohexanone;

DOI:10.1039/b406716a

Reference yield:

Ethyl protocatechuate (3943-89-3) → ethyl 3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoate (844697-16-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 30 percent / K₂CO₃ / cyclohexanone / 8 h / 70 °C

2: 57 percent / K₂CO₃; KI / cyclohexanone / 10 h / 145 °C

With potassium carbonate; potassium iodide; In cyclohexanone;

DOI:10.1039/b406716a

upstream raw materials:

2-[4-(6-bromohexyloxy)phenyl]-5-octylpyrimidine

ethyl 4-hydroxy-3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}benzoate

1 ,6-dibromohexane

Ethyl protocatechuate

Downstream raw materials:

3-{6-[2-(4-octylphenyl)pyrimidin-5-yloxy]hexyloxy}-4-{6-[4-(5-octylpyrimidin-2-yl)phenyloxy]hexyloxy}benzoic acid

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