4-methoxyphenyl 4-vinylphenyl methanone

Base Information

• Chemical Name: 4-methoxyphenyl 4-vinylphenyl methanone
• CAS No.: 24993-90-6
• Molecular Formula: C₁₆H₁₄O₂
• Molecular Weight: 238.286
• Mol file: 24993-90-6.mol

Synonyms:4-methoxyphenyl 4-vinylphenyl methanone

Chemical Property of 4-methoxyphenyl 4-vinylphenyl methanone

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-methoxyphenyl 4-vinylphenyl methanone

There total 4 articles about 4-methoxyphenyl 4-vinylphenyl methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

carbon monoxide (201230-82-2) + para-iodoanisole (696-62-8) + 4-Vinylphenylboronic acid (2156-04-9,593231-72-2) → 4-methoxyphenyl 4-vinylphenyl methanone (24993-90-6)

Guidance literature:

With C₁₂H₁₇Cl₂NO₃PPd; potassium carbonate; In 1,4-dioxane; at 100 ℃; for 2h; under 760.051 Torr; Schlenk technique;

DOI:10.1002/cctc.201700946

Reference yield:

1-bromo-4-methoxy-benzene (104-92-7) + carbon monoxide (201230-82-2) + 4-Vinylphenylboronic acid (2156-04-9,593231-72-2) → 4-methoxyphenyl 4-vinylphenyl methanone (24993-90-6)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; Hexadecane; palladium diacetate; catacxium A; In toluene; at 100 ℃; for 24h; under 1875.19 Torr; Autoclave; Inert atmosphere;

DOI:10.1002/chem.200800001

Reference yield:

1-bromo-4-methoxy-benzene (104-92-7) + carbon monoxide (201230-82-2) + 4-Vinylphenylboronic acid (2156-04-9,593231-72-2) → 4-methoxyphenyl 4-vinylphenyl methanone (24993-90-6) + 4-methoxy-4'-vinyl-1,1'-biphenyl (2782-23-2)

Guidance literature:

With Hexadecane; palladium diacetate; triethylamine; catacxium A; In toluene; at 100 ℃; for 24h; under 3750.38 Torr; Autoclave; Inert atmosphere;

DOI:10.1002/chem.200800001

upstream raw materials:

1-bromo-4-methoxy-benzene

carbon monoxide

4-Vinylphenylboronic acid

para-iodoanisole