9-benzoyl-(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one

Base Information

Chemical Name:9-benzoyl-(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one
CAS No.:1415026-87-7
Molecular Formula:C₂₆H₂₂N₂O₄
Molecular Weight:426.472
Hs Code.:

Synonyms:9-benzoyl-(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-benzoyl-(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one

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Technology Process of 9-benzoyl-(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one

There total 4 articles about 9-benzoyl-(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 918665-78-8
C₂₆H₂₄N₂O₄

: 1415026-87-7
9-benzoyl-(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one

: 1415026-94-6
(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one

Guidance literature:: With palladium(II) trifluoroacetate; oxygen; copper diacetate; In dimethyl sulfoxide; at 70 - 80 ℃; for 42h; Reagent/catalyst; Temperature; Time;
DOI:10.1016/j.tet.2012.10.011 DOI:10.1016/j.tet.2012.10.011

Reference yield:

: 10172-51-7
6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline

: 1415026-87-7
9-benzoyl-(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one

: 1415026-94-6
(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / Reflux

2: palladium(II) trifluoroacetate; copper diacetate; silver trifluoroacetate / dimethyl sulfoxide / 24 h / 100 °C / Inert atmosphere

With palladium(II) trifluoroacetate; copper diacetate; silver trifluoroacetate; In dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.tet.2012.10.011 DOI:10.1016/j.tet.2012.10.011

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 1415026-87-7
9-benzoyl-(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one

: 1415026-94-6
(2,3-dimethoxyl)-5,6,7,9-tetrahydroindolo[2,3-e][3]benzazocin-8-one

Guidance literature:: Multi-step reaction with 3 steps

2: acetonitrile / Reflux

3: palladium(II) trifluoroacetate; copper diacetate; silver trifluoroacetate / dimethyl sulfoxide / 24 h / 100 °C / Inert atmosphere

With palladium(II) trifluoroacetate; copper diacetate; silver trifluoroacetate; In dimethyl sulfoxide; acetonitrile; 1: |Bischler-Napieralski Reaction;
DOI:10.1016/j.tet.2012.10.011 DOI:10.1016/j.tet.2012.10.011