N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester

Base Information

Chemical Name:N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester
CAS No.:87010-59-1
Molecular Formula:C₁₉H₂₁Cl₃NO₅P
Molecular Weight:480.712
Hs Code.:

Synonyms:N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester

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Chemical Property of N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester

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Technology Process of N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester

There total 3 articles about N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 67942-83-0
N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester

: 122-51-0
orthoformic acid triethyl ester

: 87010-59-1
N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester

Guidance literature:: at 80 - 145 ℃;

Reference yield:

: 53558-70-6
α-(N-benzyloxycarbonyl)amino-benzylphosphonic acid

: 87010-59-1
N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / trichloroacetonitrile / pyridine / 6 h / 100 °C

2: 89 percent / 80 - 145 °C

With trichloroacetonitrile; In pyridine;

Reference yield:

: 87010-58-0
N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester

: 87010-59-1
N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / LiBr / pyridine / 2 h / 100 °C

2: 89 percent / 80 - 145 °C

With lithium bromide; In pyridine;