N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester

Base Information

• Chemical Name: N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester
• CAS No.: 67942-83-0
• Molecular Formula: C₁₇H₁₇Cl₃NO₅P
• Molecular Weight: 452.658

Synonyms:N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester

Chemical Property of N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester

There total 3 articles about N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester (87010-58-0) → N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester (67942-83-0)

Guidance literature:

With lithium bromide; In pyridine; at 100 ℃; for 2h;

Reference yield: 91.0%

1,1,1-trichloroethanol (115-20-8) + α-(N-benzyloxycarbonyl)amino-benzylphosphonic acid (53558-70-6) → N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester (67942-83-0)

Guidance literature:

With trichloroacetonitrile; In pyridine; at 100 ℃; for 6h;

Reference yield: 90.0%

N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester (87010-59-1) → N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester (67942-83-0)

Guidance literature:

With lithium bromide; In pyridine; at 100 ℃; for 2h;

upstream raw materials:

1,1,1-trichloroethanol

α-(N-benzyloxycarbonyl)amino-benzylphosphonic acid

N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester

N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester

Downstream raw materials:

N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester

N-benzyloxycarbonyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester

(Amino-phenyl-methyl)-phosphonic acid ethyl ester 2,2,2-trichloro-ethyl ester; hydrochloride

(Amino-phenyl-methyl)-phosphonic acid methyl ester 2,2,2-trichloro-ethyl ester; hydrochloride

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