Technology Process of C23H35NO6
There total 11 articles about C23H35NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
((2S,3R,4S)-1-hydroxy-2,4-dimethyldecan-3-yl) (S)-2-(benzyloxycarbonylamino)propanoate;
With
pyridine-SO3 complex;
In
dichloromethane; dimethyl sulfoxide;
at 0 ℃;
for 1h;
With
sodium chlorite; sodium dihydrogenphosphate;
In
tert-butyl alcohol;
Further stages.;
DOI:10.1016/j.tetlet.2008.03.107
- Guidance literature:
-
With
sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene;
In
water; tert-butyl alcohol;
at 20 ℃;
for 1h;
DOI:10.1016/j.tetasy.2013.07.012
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: sodium periodate / tetrahydrofuran; water / 2 h / 0 - 20 °C
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C
2.2: 0.5 h / 0 °C
3.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 760.05 Torr
4.1: 1H-imidazole / tetrahydrofuran / 8 h / 0 °C
5.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 5 h / 0 - 20 °C
6.1: camphor-10-sulfonic acid / methanol; dichloromethane / 0.5 h / 0 °C
7.1: triethylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
8.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate dihydrate / water; tert-butyl alcohol / 1 h / 20 °C
With
1H-imidazole; dmap; sodium chlorite; sodium periodate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; palladium 10% on activated carbon; camphor-10-sulfonic acid; hydrogen; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;
2.1: |Wittig Olefination / 2.2: |Wittig Olefination / 7.1: |Parikh-Doering Oxidation;
DOI:10.1016/j.tetasy.2013.07.012
