ethylthio(triphenylsilyl)keten

Base Information

Chemical Name:ethylthio(triphenylsilyl)keten
CAS No.:98014-97-2
Molecular Formula:C₂₂H₂₀OSSi
Molecular Weight:360.552
Hs Code.:

Synonyms:ethylthio(triphenylsilyl)keten

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethylthio(triphenylsilyl)keten

Chemical Property:

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Technology Process of ethylthio(triphenylsilyl)keten

There total 7 articles about ethylthio(triphenylsilyl)keten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: (CO)5WC(SEt)SiPh₃

: 98014-96-1
(CO)5W(SEt)C(SiPh₃)=C=O

: 98014-97-2
ethylthio(triphenylsilyl)keten

Guidance literature:: With carbon monoxide; In pentane; under nitrogen; vigorous stream of CO is passed through solution (6 h) at 20 °C;; identification by spectroscopy; isolation of ethylthio(triphenylsilyl)ketene;;
DOI:10.1016/0022-328X(88)89026-0

Reference yield:

: 98014-96-1
(CO)5W(SEt)C(SiPh₃)=C=O

: 14040-11-0
tungsten hexacarbonyl

: 98014-97-2
ethylthio(triphenylsilyl)keten

Guidance literature:: With carbon monoxide; In diethyl ether; under nitrogen; autoclave; 50 atm; 1 hour at 80 - 100 °C;;
DOI:10.1016/0022-328X(88)89026-0

Reference yield:

: C₂₂H₂₀OSSiW*5CO

: 98014-97-2
ethylthio(triphenylsilyl)keten

Guidance literature:: With triethylamine hydrochloride; In dichloromethane; for 1h; Yield given; Ambient temperature;
DOI:10.1016/0022-328X(88)89026-0