2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose

Base Information

Chemical Name:2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose
CAS No.:74293-23-5
Molecular Formula:C₅₁H₅₁NO₁₀
Molecular Weight:837.967
Hs Code.:

2,3,4,6-tetra-O-benzyl-1-O-<N-benzyloxycarbonyl-L-tyrosyl>-α-D-glucopyranose

Synonyms:2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose

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Chemical Property of 2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose

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Technology Process of 2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose

There total 3 articles about 2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 74293-21-3
2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose

: 74293-23-5
2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose

Guidance literature:: With trifluoroacetic acid; at -10 ℃; for 1h;
DOI:10.1016/S0008-6215(00)85315-X

Reference yield:

: 5545-54-0
N-(benzyloxycarbonyl)-O-(1,1-dimethylethyl)-L-tyrosine

: 74293-23-5
2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / DCC / ethyl acetate

2: 300 mg / imidazole / CH₂Cl₂ / 24 h / Ambient temperature

3: 53 percent / trifluoroacetic acid / 1 h / -10 °C

With 1H-imidazole; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate;
DOI:10.1016/S0008-6215(00)85315-X

Reference yield:

: 74293-19-9
N-benzyloxycarbonyl-O-(tert-butyl)-L-tyrosine p-nitrophenyl ester

: 74293-23-5
2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 300 mg / imidazole / CH₂Cl₂ / 24 h / Ambient temperature

2: 53 percent / trifluoroacetic acid / 1 h / -10 °C

With 1H-imidazole; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0008-6215(00)85315-X