H-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt

Base Information

Chemical Name:H-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt
CAS No.:133851-96-4
Molecular Formula:C₂HF₃O₂*C₁₇H₂₆N₄O₃
Molecular Weight:448.442
Hs Code.:

H-Gly-Phe-Leu-NH<sub>2</sub> trifluoroacetic acid salt

Synonyms:H-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt

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Chemical Property of H-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt

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Technology Process of H-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt

There total 1 articles about H-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4530-20-5
BOC-glycine

: 76-05-1
trifluoroacetic acid

: H-Phe-Leu-NH₂ trifluoroacetic acid salt

: 133851-96-4
H-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt

Guidance literature:: BOC-glycine; H-Phe-Leu-NH₂ trifluoroacetic acid salt; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;

trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h; Further stages.;
DOI:10.1021/ol701817u

Reference yield:

: 4530-20-5
BOC-glycine

: 133851-96-4
H-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt

: 76-05-1
trifluoroacetic acid

: H-Gly-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt

Guidance literature:: BOC-glycine; H-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;

trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h; Further stages.;
DOI:10.1021/ol701817u

Reference yield:

: 133851-88-4
Z-Tyr(Bzl)Ψ(CH2O)Gly-OH

: 133851-96-4
H-Gly-Phe-Leu-NH₂ trifluoroacetic acid salt

: 133851-89-5
Z-Tyr(Bzl)-Ψ(CH2O)Gly-Gly-Phe-Leu-NH2

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; Yield given. Multistep reaction; 1.) DMF, -25 deg C, 5 min, 2.) DMF, -20 deg C;
DOI:10.1021/jm00112a018