2-(4-amino-3-cyclohex-1-enyl-phenyl)-ethanesulfonic acid tert-butylamide

Base Information

Chemical Name:2-(4-amino-3-cyclohex-1-enyl-phenyl)-ethanesulfonic acid tert-butylamide
CAS No.:915006-40-5
Molecular Formula:C₁₈H₂₈N₂O₂S
Molecular Weight:336.499
Hs Code.:

Synonyms:2-(4-amino-3-cyclohex-1-enyl-phenyl)-ethanesulfonic acid tert-butylamide

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Chemical Property of 2-(4-amino-3-cyclohex-1-enyl-phenyl)-ethanesulfonic acid tert-butylamide

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Technology Process of 2-(4-amino-3-cyclohex-1-enyl-phenyl)-ethanesulfonic acid tert-butylamide

There total 5 articles about 2-(4-amino-3-cyclohex-1-enyl-phenyl)-ethanesulfonic acid tert-butylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 915006-40-5
2-(4-amino-3-cyclohex-1-enyl-phenyl)-ethanesulfonic acid tert-butylamide

Guidance literature:

Reference yield:

: 915006-37-0
2-(4-amino-3-bromo-phenyl)-ethanesulfonic acid tert-butylamide

: 89490-05-1,21190-87-4
cyclohex-1-enylboronic acid

: 915006-40-5
2-(4-amino-3-cyclohex-1-enyl-phenyl)-ethanesulfonic acid tert-butylamide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; water; at 80 ℃; for 5h;
DOI:10.1016/j.bmcl.2013.09.061

Reference yield:

: 915006-38-1
2-(4-nitro-phenyl)-ethanesulfonic acid tert-butylamide

: 915006-40-5
2-(4-amino-3-cyclohex-1-enyl-phenyl)-ethanesulfonic acid tert-butylamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; palladium 10% on activated carbon / ethyl acetate / 6 h

2: N-Bromosuccinimide / dichloromethane / 1 h / 0 - 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,4-dioxane / 5 h / 80 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; sodium carbonate; In 1,4-dioxane; dichloromethane; water; ethyl acetate; 3: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.bmcl.2013.09.061