2(1H)-Pyrimidinone, 4,6-dimethyl-, oxime (9CI)

Base Information

• Chemical Name: 2(1H)-Pyrimidinone, 4,6-dimethyl-, oxime (9CI)
• CAS No.: 89808-15-1
• Molecular Formula: C6H9 N3 O
• Molecular Weight: 139.157
• Hs Code.: 2933599090
• Mol file: 89808-15-1.mol

Synonyms:2(1H)-Pyrimidinone,4,6-dimethyl-, oxime (9CI); Pyrimidine, 2-hydroxyamino-4,6-dimethyl- (6CI)

Chemical Property of 2(1H)-Pyrimidinone, 4,6-dimethyl-, oxime (9CI)

Chemical Property:

• PSA: 61.27000
• LogP: 0.31640

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2(1H)-Pyrimidinone, 4,6-dimethyl-, oxime (9CI)

There total 4 articles about 2(1H)-Pyrimidinone, 4,6-dimethyl-, oxime (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-chloro-4,6-dimethylpyrimidine (4472-44-0) → 2-Hydroxyamino-4,6-dimethylpyrimidine (89808-15-1)

Guidance literature:

With hydroxylamine hydrochloride; triethylamine; In ethanol; at 90 ℃; Reflux;

DOI:10.1021/jacs.5b11273

Reference yield: 68.0%

2-chloro-4,6-dimethylpyrimidine (4472-44-0) → 4,6-dimethylpirimidin-2-one (108-79-2) + 2-Hydroxyamino-4,6-dimethylpyrimidine (89808-15-1)

Guidance literature:

With hydroxylamine hydrochloride; triethylamine; In ethanol; for 3.5h; Heating;

DOI:10.1007/BF00471808

Reference yield:

(4,6-dimethyl-pyrimidin-2-yl)-nitro-amine (99418-09-4) → 2-Hydroxyamino-4,6-dimethylpyrimidine (89808-15-1)

Guidance literature:

With hydroxylamine;

upstream raw materials:

(4,6-dimethyl-pyrimidin-2-yl)-nitro-amine

2-chloro-4,6-dimethylpyrimidine

acetylacetone

Downstream raw materials:

C₁₃H₁₃N₃O₂

C₁₃H₁₁Cl₂N₃O₂

4,6-dimethyl-2-nitrosopyrimidine

(4,6-Dimethyl-pyrimidin-2-yl)-phenyl-diazene

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