C₅₉H₄₃N₃OS₂

Base Information

• Chemical Name: C₅₉H₄₃N₃OS₂
• CAS No.: 1361587-78-1
• Molecular Formula: C₅₉H₄₃N₃OS₂
• Molecular Weight: 874.142
• Mol file: 1361587-78-1.mol

Synonyms:C₅₉H₄₃N₃OS₂

Chemical Property of C₅₉H₄₃N₃OS₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₉H₄₃N₃OS₂

There total 4 articles about C₅₉H₄₃N₃OS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

p-(5-(tributylstannyl)thiophen-2-yl)-N-(phenyl)-N-(naphthalen-1-yl)phenylamine (1378024-65-7) + C33H25BrN2OS (1361587-81-6) → C59H43N3OS2 (1361587-78-1)

Guidance literature:

With trans-bis(triphenylphosphine)palladium dichloride; In N,N-dimethyl-formamide; at 90 ℃; Inert atmosphere;

DOI:10.1039/c2jm13961h

Reference yield:

N-(4-(10H-phenothiazine-10-yl)phenyl)-4-methyl-N-(p-tolyl)aniline (1378024-76-0) → C59H43N3OS2 (1361587-78-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / Inert atmosphere

2.2: Inert atmosphere

3.1: trans-bis(triphenylphosphine)palladium dichloride / N,N-dimethyl-formamide / 90 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; trans-bis(triphenylphosphine)palladium dichloride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c2jm13961h

Reference yield:

10H-phenothiazine (92-84-2) → C59H43N3OS2 (1361587-78-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium t-butanolate / toluene / 15 h / 90 °C / Inert atmosphere

2.1: N-Bromosuccinimide / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / Inert atmosphere

3.2: Inert atmosphere

4.1: trans-bis(triphenylphosphine)palladium dichloride / N,N-dimethyl-formamide / 90 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; N-Bromosuccinimide; n-butyllithium; trans-bis(triphenylphosphine)palladium dichloride; palladium diacetate; sodium t-butanolate; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1039/c2jm13961h

upstream raw materials:

p-(5-(tributylstannyl)thiophen-2-yl)-N-(phenyl)-N-(naphthalen-1-yl)phenylamine

C₃₃H₂₅BrN₂OS

N-(4-(10H-phenothiazine-10-yl)phenyl)-4-methyl-N-(p-tolyl)aniline

10H-phenothiazine

Downstream raw materials:

C₆₂H₄₄N₄O₂S₂