(R)-3-fluoro-2-[2-chloro-5-(5-oxo-pyrrolidin-3-yl)-phenoxy]-benzonitrile

Base Information

• Chemical Name: (R)-3-fluoro-2-[2-chloro-5-(5-oxo-pyrrolidin-3-yl)-phenoxy]-benzonitrile
• CAS No.: 903579-11-3
• Molecular Formula: C₁₇H₁₂ClFN₂O₂
• Molecular Weight: 330.746

Synonyms:(R)-3-fluoro-2-[2-chloro-5-(5-oxo-pyrrolidin-3-yl)-phenoxy]-benzonitrile

Chemical Property of (R)-3-fluoro-2-[2-chloro-5-(5-oxo-pyrrolidin-3-yl)-phenoxy]-benzonitrile

Chemical Property:

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Technology Process of (R)-3-fluoro-2-[2-chloro-5-(5-oxo-pyrrolidin-3-yl)-phenoxy]-benzonitrile

There total 1 articles about (R)-3-fluoro-2-[2-chloro-5-(5-oxo-pyrrolidin-3-yl)-phenoxy]-benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-4-(4-chloro-3-hydroxy-phenyl)-pyrrolidin-2-one + 2,3-difluorobenzonitrile (21524-39-0) → (R)-3-fluoro-2-[2-chloro-5-(5-oxo-pyrrolidin-3-yl)-phenoxy]-benzonitrile (903579-11-3)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 20 ℃; for 24h;

Reference yield:

(R)-3-fluoro-2-[2-chloro-5-(5-oxo-pyrrolidin-3-yl)-phenoxy]-benzonitrile (903579-11-3) + 4-bromo-N,N-bis-(4-methoxybenzyl)-2-(4-methoxy-benzylamino)-benzenesulfonamide (903578-47-2) → 4-{4-[4-chloro-3-(2-cyano-6-fluoro-phenoxy)-phenyl]-2-oxo-pyrrolidin-1-yl}-N,N-bis-(4-methoxy-benzyl)-2-(4-methoxy-benzylamino)-benzenesulfonamide

Guidance literature:

With potassium phosphate; (±)-trans-1,2-diaminocyclohexane; copper(l) iodide; In 1,4-dioxane; N,N-dimethyl-formamide; at 110 ℃; for 20h;

upstream raw materials:

2,3-difluorobenzonitrile

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