2-(p-nitrophenylhydrazono)-2-cyan-N,N-(3-oxopentamethylen)-acetamidin

Base Information

• Chemical Name: 2-(p-nitrophenylhydrazono)-2-cyan-N,N-(3-oxopentamethylen)-acetamidin
• CAS No.: 134425-87-9
• Molecular Formula: C₁₃H₁₄N₆O₃
• Molecular Weight: 302.293
• Mol file: 134425-87-9.mol

Synonyms:2-(p-nitrophenylhydrazono)-2-cyan-N,N-(3-oxopentamethylen)-acetamidin

Chemical Property of 2-(p-nitrophenylhydrazono)-2-cyan-N,N-(3-oxopentamethylen)-acetamidin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(p-nitrophenylhydrazono)-2-cyan-N,N-(3-oxopentamethylen)-acetamidin

There total 1 articles about 2-(p-nitrophenylhydrazono)-2-cyan-N,N-(3-oxopentamethylen)-acetamidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

morpholine (110-91-8,99108-56-2) + 4-nitrophenylhydrazonopropanedinitrile (3722-12-1) → 2-(p-nitrophenylhydrazono)-2-cyan-N,N-(3-oxopentamethylen)-acetamidin (134425-87-9)

Guidance literature:

In methanol; for 0.5h; Heating;

DOI:10.1007/BF00809365

Reference yield: 76.0%

2-(p-nitrophenylhydrazono)-2-cyan-N,N-(3-oxopentamethylen)-acetamidin (134425-87-9) → 2-(4-nitrophenyl)-4-cyano-5-morpholino-1-yl-2H-[1,2,3]triazole (134425-95-9)

Guidance literature:

With pyridine; copper (I) acetate; at 110 ℃; for 0.5h;

DOI:10.1007/BF00809365

Reference yield: 65.0%

2-(p-nitrophenylhydrazono)-2-cyan-N,N-(3-oxopentamethylen)-acetamidin (134425-87-9) + chloroacetyl chloride (79-04-9) → 2-(p-nitrophenylhydrazono)-2-cyan-N-chloracetyl-acetamid (134426-09-8)

Guidance literature:

With potassium carbonate; In 1,4-dioxane; at 60 ℃; for 2h;

DOI:10.1007/BF00809365

upstream raw materials:

morpholine

4-nitrophenylhydrazonopropanedinitrile

Downstream raw materials:

2-(4-nitrophenyl)-4-cyano-5-morpholino-1-yl-2H-[1,2,3]triazole

2-(p-nitrophenylhydrazono)-2-cyan-N-chloracetyl-acetamid

4-amino-2,6-dioxo-5-(p-nitrophenylhydrazono)-1,2,5,6-tetrahydropyrid-3-yl-pyridiniumchlorid