C₅₅H₅₁ClF₂N₂O₂₃

Base Information

Chemical Name:C₅₅H₅₁ClF₂N₂O₂₃
CAS No.:1292322-45-2
Molecular Formula:C₅₅H₅₁ClF₂N₂O₂₃
Molecular Weight:1181.46
Hs Code.:

C<sub>55</sub>H<sub>51</sub>ClF<sub>2</sub>N<sub>2</sub>O<sub>23</sub>

Synonyms:C₅₅H₅₁ClF₂N₂O₂₃

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Chemical Property of C₅₅H₅₁ClF₂N₂O₂₃

Chemical Property:

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Technology Process of C₅₅H₅₁ClF₂N₂O₂₃

There total 11 articles about C₅₅H₅₁ClF₂N₂O₂₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 590-97-6
acetoxymethyl bromide

: C₄₀H₂₆ClF₂N₂O₁₃^(5-)*5K⁽¹⁺⁾

: 1292322-45-2
C₅₅H₅₁ClF₂N₂O₂₃

Guidance literature:: C₄₀H₂₆ClF₂N₂O₁₃^(5-)*5K⁽¹⁺⁾; With hydrogenchloride; In water; pH=1.5;

acetoxymethyl bromide; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 2437-17-4
6-hydroxy-1-naphthoic acid

: 1292322-45-2
C₅₅H₅₁ClF₂N₂O₂₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: sulfuric acid / 80 °C

2.1: Selectfluor / acetonitrile / 3 h / 20 °C

3.1: zinc; acetic acid

4.1: SEC-BUTYLAMINE; sulfuryl dichloride / toluene / 3 h / 66 °C

5.1: potassium carbonate / acetonitrile / 2 h / Reflux

6.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h

7.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

8.1: 3-chloro-benzenecarboperoxoic acid; potassium hydroxide / benzene / 24 h / 70 °C

9.1: boron tribromide / dichloromethane / 3 h

9.2: Cooling with ice

10.1: methanesulfonic acid

10.3: 0.5 h / 20 °C

11.1: hydrogenchloride / water / pH 1.5

11.2: 2 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; sulfuryl dichloride; SEC-BUTYLAMINE; methanesulfonic acid; sulfuric acid; boron tribromide; potassium carbonate; acetic acid; Selectfluor; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; potassium hydroxide; zinc; In diethyl ether; dichloromethane; water; toluene; acetonitrile; benzene; 8.1: Baeyer-Villager;

Reference yield:

: 90162-13-3
methyl 6-hydroxy-1-naphthoate

: 1292322-45-2
C₅₅H₅₁ClF₂N₂O₂₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: Selectfluor / acetonitrile / 3 h / 20 °C

2.1: zinc; acetic acid

3.1: SEC-BUTYLAMINE; sulfuryl dichloride / toluene / 3 h / 66 °C

4.1: potassium carbonate / acetonitrile / 2 h / Reflux

5.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h

6.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

7.1: 3-chloro-benzenecarboperoxoic acid; potassium hydroxide / benzene / 24 h / 70 °C

8.1: boron tribromide / dichloromethane / 3 h

8.2: Cooling with ice

9.1: methanesulfonic acid

9.3: 0.5 h / 20 °C

10.1: hydrogenchloride / water / pH 1.5

10.2: 2 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; sulfuryl dichloride; SEC-BUTYLAMINE; methanesulfonic acid; boron tribromide; potassium carbonate; acetic acid; Selectfluor; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; potassium hydroxide; zinc; In diethyl ether; dichloromethane; water; toluene; acetonitrile; benzene; 7.1: Baeyer-Villager;