N-[(1-tert-butyl-1H-1,2,3-triazol-4-yl)methylene]-N-phenylamine

Base Information

Chemical Name:N-[(1-tert-butyl-1H-1,2,3-triazol-4-yl)methylene]-N-phenylamine
CAS No.:133902-59-7
Molecular Formula:C₁₃H₁₆N₄
Molecular Weight:228.297
Hs Code.:
Mol file:133902-59-7.mol

Synonyms:[1-(1-tert-Butyl-1H-[1,2,3]triazol-4-yl)-meth-(E)-ylidene]-phenyl-amine

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Chemical Property of N-[(1-tert-butyl-1H-1,2,3-triazol-4-yl)methylene]-N-phenylamine

Chemical Property:

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Technology Process of N-[(1-tert-butyl-1H-1,2,3-triazol-4-yl)methylene]-N-phenylamine

There total 11 articles about N-[(1-tert-butyl-1H-1,2,3-triazol-4-yl)methylene]-N-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 133902-47-3
tert-Butyl-[1-(1-phenyl-1H-[1,2,3]triazol-4-yl)-meth-(E)-ylidene]-amine

: 133902-59-7
[1-(1-tert-Butyl-1H-[1,2,3]triazol-4-yl)-meth-(E)-ylidene]-phenyl-amine

Guidance literature:: In dimethyl sulfoxide; at 80 ℃;

Reference yield:

: 1516-60-5
4-nitrophenyl azide

: 133902-59-7
[1-(1-tert-Butyl-1H-[1,2,3]triazol-4-yl)-meth-(E)-ylidene]-phenyl-amine

Guidance literature:: Multi-step reaction with 7 steps

1: 71 percent / toluene / Heating

2: 36 percent / NaBH₄ / methanol / 1 h / Heating

3: 47 percent / MnO₂ / CH₂Cl₂ / Ambient temperature

4: 51 percent / ethanol / Ambient temperature

5: 2) HCOOH / 1) 80 deg C, DMSO, overnight, 2) H₂O, MeOH, reflux, 12 h

6: 93 percent / methanol / Ambient temperature

7: 74 percent / dimethylsulfoxide / 80 °C

With manganese(IV) oxide; sodium tetrahydroborate; formic acid; In methanol; ethanol; dichloromethane; dimethyl sulfoxide; toluene;

Reference yield:

: 103755-58-4
(1-phenyl-1H-1,2,3-triazole-4-yl)methanol

: 133902-59-7
[1-(1-tert-Butyl-1H-[1,2,3]triazol-4-yl)-meth-(E)-ylidene]-phenyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / MnO₂ / CH₂Cl₂ / Ambient temperature

2: 93 percent / methanol / Ambient temperature

3: 74 percent / dimethylsulfoxide / 80 °C

With manganese(IV) oxide; In methanol; dichloromethane; dimethyl sulfoxide;