1-azido-4-(p-carboxyphenoxy)-2-butanone ethylene ketal

Base Information

Chemical Name:1-azido-4-(p-carboxyphenoxy)-2-butanone ethylene ketal
CAS No.:78520-75-9
Molecular Formula:C₁₃H₁₅N₃O₅
Molecular Weight:293.279
Hs Code.:

Synonyms:1-azido-4-(p-carboxyphenoxy)-2-butanone ethylene ketal

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Chemical Property of 1-azido-4-(p-carboxyphenoxy)-2-butanone ethylene ketal

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Technology Process of 1-azido-4-(p-carboxyphenoxy)-2-butanone ethylene ketal

There total 3 articles about 1-azido-4-(p-carboxyphenoxy)-2-butanone ethylene ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

: 78520-74-8
1-azido-4--2-butanone ethylene ketal

: 78520-75-9
1-azido-4-(p-carboxyphenoxy)-2-butanone ethylene ketal

Guidance literature:: With sodium hydroxide; In acetonitrile; for 18h; Ambient temperature;
DOI:10.1021/jm00141a010

Reference yield:

: 78520-73-7
1-azido-4--2-butanone

: 78520-75-9
1-azido-4-(p-carboxyphenoxy)-2-butanone ethylene ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / p-toluenesulfonic acid monohydrate / benzene / 6 h / Heating

2: 93.5 percent / 0.5 N NaOH / acetonitrile / 18 h / Ambient temperature

With sodium hydroxide; toluene-4-sulfonic acid; In acetonitrile; benzene;
DOI:10.1021/jm00141a010

Reference yield:

: 72155-10-3
1-bromo-4-2-butanone

: 78520-75-9
1-azido-4-(p-carboxyphenoxy)-2-butanone ethylene ketal

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / sodium azide, potassium iodide / acetone / 2 h

2: 82 percent / p-toluenesulfonic acid monohydrate / benzene / 6 h / Heating

3: 93.5 percent / 0.5 N NaOH / acetonitrile / 18 h / Ambient temperature

With sodium hydroxide; sodium azide; toluene-4-sulfonic acid; potassium iodide; In acetone; acetonitrile; benzene;
DOI:10.1021/jm00141a010