2-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenylcarbamoyl]-benzenesulfonic acid

Base Information

Chemical Name:2-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenylcarbamoyl]-benzenesulfonic acid
CAS No.:124778-86-5
Molecular Formula:C₂₃H₂₆ClN₃O₅S
Molecular Weight:491.996
Hs Code.:

Synonyms:2-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenylcarbamoyl]-benzenesulfonic acid

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Chemical Property of 2-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenylcarbamoyl]-benzenesulfonic acid

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Technology Process of 2-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenylcarbamoyl]-benzenesulfonic acid

There total 5 articles about 2-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenylcarbamoyl]-benzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114799-96-1
2-n-butyl-4-chloro-5-(methoxymethyl)-1-<(4-nitrophenyl)methyl>imidazole

: 124778-86-5
2-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenylcarbamoyl]-benzenesulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 56.5 percent / H₂ / 10percent Pd/C / methanol / 4 h

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00167a007

Reference yield:

: 114799-92-7
2-Butyl-4-chloro-1-[(4-nitrophenyl)methyl]-1H-imidazole-5-methanol

: 124778-86-5
2-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenylcarbamoyl]-benzenesulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 11.57 g / concd. sulfuric acid / Heating

2: 56.5 percent / H₂ / 10percent Pd/C / methanol / 4 h

With sulfuric acid; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00167a007

Reference yield:

: 79047-41-9
2-n-butyl-4-chloro-5-hydroxymethylimidazole

: 124778-86-5
2-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenylcarbamoyl]-benzenesulfonic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium methoxide / 1.) methanol, 0 deg C, 2.) DMF, 25 deg C

2: 11.57 g / concd. sulfuric acid / Heating

3: 56.5 percent / H₂ / 10percent Pd/C / methanol / 4 h

With sulfuric acid; hydrogen; sodium methylate; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00167a007