[palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)]

Base Information

Chemical Name:[palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)]
CAS No.:773887-40-4
Molecular Formula:C₁₂H₂₁IN₂OPd
Molecular Weight:442.636
Hs Code.:

[palladium(2-(OH)C<sub>6</sub>H<sub>4</sub>)I(N,N,N',N'-tetramethylethylenediamine)]

Synonyms:[palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)]

Suppliers and Price of [palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of [palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)]

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

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Technology Process of [palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)]

There total 1 articles about [palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: Pd2(dba)4

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 533-58-4
2-Iodophenol

: 773887-40-4
[palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)]

Guidance literature:: In toluene; byproducts: Pd; iodophenol and diamine were added to suspn. of Pd compd. in toluene; mixt. was stirred at 0°C for 3 h under N2; evapd. (vac.); extd. (CH2Cl2); filtered over MgSO4; concd.; Et2O added; filtered; washed (Et2O); dried; elem. anal.;
DOI:10.1021/om0496131

Reference yield: 83.0%

: 773887-40-4
[palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)]

: 773-82-0
Pentafluorobenzonitrile

: 73491-36-8
thallium(I) triflate

: 869477-64-5
[palladium(1-O-2-[C(C6F5)NH]C6H4-κ2-O,N)(N,N,N',N'-tetramethylethylenediamine)]CF3SO3

Guidance literature:: In dichloromethane; C6F5CN and Tl(I) triflate added to soln. of Pd complex in CH2Cl2, mixt. stirred at room temp. for 4 h; suspn. filtered over Celite, filtrate concd., Et2O added, ppt. filtered off, washed with Et2O, dried; elem. anal.;
DOI:10.1002/anie.200501202

Reference yield: 80.0%

: 773887-40-4
[palladium(2-(OH)C₆H₄)I(N,N,N',N'-tetramethylethylenediamine)]

: 624-48-6
dimethyl cis-but-2-ene-1,4-dioate

: 73491-36-8
thallium(I) triflate

: [Pd(κ2C,O-2-[CH(CO2Me)CH(CO2Me)]C6H4OH)(N,N,N',N'-tetramethylethylenediamine)]OTf

Guidance literature:: In dichloromethane; byproducts: TlI; To soln. of palladium complex in CH2Cl2 were added maleate and TlOTf, stirred for 17 h at room temp.; filtered, concd., precipitated with Et2O, filtered, washed with Et2O, suction-dried, elem. anal.;
DOI:10.1021/om900957s