N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethyl)-N-[dimethyl(phenyl)]silylamine

Base Information

Chemical Name:N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethyl)-N-[dimethyl(phenyl)]silylamine
CAS No.:1488023-34-2
Molecular Formula:C₂₂H₂₅NSi
Molecular Weight:339.469
Hs Code.:

Synonyms:N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethyl)-N-[dimethyl(phenyl)]silylamine

Suppliers and Price of N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethyl)-N-[dimethyl(phenyl)]silylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethyl)-N-[dimethyl(phenyl)]silylamine

Chemical Property:

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Technology Process of N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethyl)-N-[dimethyl(phenyl)]silylamine

There total 3 articles about N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethyl)-N-[dimethyl(phenyl)]silylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17537-31-4
Acetophenone-methyl-d3

: 766-77-8
Dimethylphenylsilane

: 14545-23-4
aniline-d₇

: 1488023-28-4
C₁₄H₆⁽²⁾H₉N

: 1488023-33-1
C₂₂H₁₆⁽²⁾H₇NSi

: 1488023-34-2
N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethyl)-N-[dimethyl(phenyl)]silylamine

Guidance literature:: With tris(pentafluorophenyl)borate; In benzene; at 20 ℃;
DOI:10.1021/ja409344w

Reference yield:

: 17537-31-4
Acetophenone-methyl-d3

: 14545-23-4
aniline-d₇

: 1488023-34-2
N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethyl)-N-[dimethyl(phenyl)]silylamine

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 24 h / 65 °C / Molecular sieve; Inert atmosphere

2: (S)-4-(pentafluorophenyl)-4,5-dihydro-3H-dinaphtho[2,1-c:1',2'-e]borepine tetrahydrofuran / 1,2-dichloro-benzene / 20 °C

With (S)-4-(pentafluorophenyl)-4,5-dihydro-3H-dinaphtho[2,1-c:1',2'-e]borepine tetrahydrofuran; In 1,2-dichloro-benzene; toluene;
DOI:10.1021/ja409344w

Reference yield:

: 766-77-8
Dimethylphenylsilane

: 1488023-38-6
(E)-N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethylidene)amine

: 1488023-34-2
N-pentadeuteriophenyl-N-(2-trideuterio-1-phenylethyl)-N-[dimethyl(phenyl)]silylamine

Guidance literature:: With (S)-4-(pentafluorophenyl)-4,5-dihydro-3H-dinaphtho[2,1-c:1',2'-e]borepine tetrahydrofuran; In 1,2-dichloro-benzene; at 20 ℃; Reagent/catalyst;
DOI:10.1021/ja409344w