1-(o-Chlor-benzoyl)-2-anilino-2-methylthio-ethen

Base Information

• Chemical Name: 1-(o-Chlor-benzoyl)-2-anilino-2-methylthio-ethen
• CAS No.: 71504-09-1
• Molecular Formula: C₁₆H₁₄ClNOS
• Molecular Weight: 303.812

Synonyms:1-(o-Chlor-benzoyl)-2-anilino-2-methylthio-ethen

Chemical Property of 1-(o-Chlor-benzoyl)-2-anilino-2-methylthio-ethen

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Technology Process of 1-(o-Chlor-benzoyl)-2-anilino-2-methylthio-ethen

There total 2 articles about 1-(o-Chlor-benzoyl)-2-anilino-2-methylthio-ethen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1-(2-chlorophenyl)ethanone (2142-68-9) + phenyl isothiocyanate (103-72-0) + methyl iodide (74-88-4) → 1-(o-Chlor-benzoyl)-2-anilino-2-methylthio-ethen (71504-09-1)

Guidance literature:

1-(2-chlorophenyl)ethanone; phenyl isothiocyanate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

methyl iodide; for 1h;

DOI:10.1039/c1gc16129f

Reference yield: 67.0%

1-(2-chlorophenyl)-3,3-bis(methylthio)prop-2-en-1-one (56944-67-3) + aniline (62-53-3) → 1-(o-Chlor-benzoyl)-2-anilino-2-methylthio-ethen (71504-09-1)

Guidance literature:

With acidic silica supported anhydrous AlCl₃; at 60 ℃; Reagent/catalyst; Temperature; regiospecific reaction; Catalytic behavior; Green chemistry;

DOI:10.1039/c5ra21421a

Reference yield: 84.0%

1-(o-Chlor-benzoyl)-2-anilino-2-methylthio-ethen (71504-09-1) + 1,3-cylohexanedione (504-02-9) + 3-nitro-benzaldehyde (99-61-6) → 3-(2-chlorobenzoyl)-4-(3-nitrophenyl)-2-phenylamino-4,6,7,8-tetrahydrochromen-5-one (1360603-97-9)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; at 100 ℃; for 0.916667h; regioselective reaction; Neat (no solvent);

DOI:10.1039/c1gc16129f

upstream raw materials:

1-(2-chlorophenyl)ethanone

phenyl isothiocyanate

methyl iodide

1-(2-chlorophenyl)-3,3-bis(methylthio)prop-2-en-1-one

Downstream raw materials:

3-(2-chlorobenzoyl)-4-(4-nitrophenyl)-2-(phenylamino)pyrano[3,2-c]chromen-5(4H)-one

4-(4-bromophenyl)-3-(2-chlorobenzoyl)-2-phenylamino-4H-pyrano[3,2-c]chromen-5-one

7-(4-nitrophenyl)-13-phenyl-7,13-dihydro-5,14-dioxa-13-azabenzo[a]naphthacene-6,8-dione

3-(2-chlorobenzoyl)-4-(3-nitrophenyl)-2-phenylamino-4,6,7,8-tetrahydrochromen-5-one

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