5-Pyrimidinecarboxylic acid, 1,4-dihydro-2-methyl-4-thioxo- (9CI)

Base Information

Chemical Name:5-Pyrimidinecarboxylic acid, 1,4-dihydro-2-methyl-4-thioxo- (9CI)
CAS No.:89640-71-1
Molecular Formula:C₆H₆N₂O₂S
Molecular Weight:170.192
Hs Code.:2933599090
Mol file:89640-71-1.mol

Synonyms:5-Pyrimidinecarboxylicacid, 1,4-dihydro-2-methyl-4-thioxo- (9CI); 5-Pyrimidinecarboxylic acid, 4-mercapto-2-methyl-(6CI,7CI)

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Pyrimidinecarboxylic acid, 1,4-dihydro-2-methyl-4-thioxo- (9CI)

Chemical Property:

PSA：101.88000
LogP:0.77190

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Pyrimidinecarboxylic acid, 1,4-dihydro-2-methyl-4-thioxo- (9CI)

There total 3 articles about 5-Pyrimidinecarboxylic acid, 1,4-dihydro-2-methyl-4-thioxo- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2134-37-4
2-methyl-6-thioxo-1,6-dihydro-pyrimidine-5-carboxylic acid ethyl ester

: 89640-71-1
2-methyl-6-thioxo-1,6-dihydro-pyrimidine-5-carboxylic acid

Guidance literature:: With sodium hydroxide;

Reference yield:

: 2134-36-3
ethyl 4-chloro-2-methylpyrimidine-5-carboxylate

: 89640-71-1
2-methyl-6-thioxo-1,6-dihydro-pyrimidine-5-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: NaHS

2: aqueous NaOH

With sodium hydroxide; sodium hydrogensulfide;

Reference yield:

: 53135-24-3
ethyl 3,4-dihydro-4-oxo-2-methylpyrimidine-5-carboxylate

: 89640-71-1
2-methyl-6-thioxo-1,6-dihydro-pyrimidine-5-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: POCl₃

2: NaHS

3: aqueous NaOH

With sodium hydroxide; sodium hydrogensulfide; trichlorophosphate;