1-(((2S,3S)-2-(benzyloxy)-5-methylhex-5-en-3-yloxy)methyl)-4-methoxybenzene

Base Information

Chemical Name:1-(((2S,3S)-2-(benzyloxy)-5-methylhex-5-en-3-yloxy)methyl)-4-methoxybenzene
CAS No.:1352481-37-8
Molecular Formula:C₂₂H₂₈O₃
Molecular Weight:340.463
Hs Code.:

Synonyms:1-(((2S,3S)-2-(benzyloxy)-5-methylhex-5-en-3-yloxy)methyl)-4-methoxybenzene

Suppliers and Price of 1-(((2S,3S)-2-(benzyloxy)-5-methylhex-5-en-3-yloxy)methyl)-4-methoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(((2S,3S)-2-(benzyloxy)-5-methylhex-5-en-3-yloxy)methyl)-4-methoxybenzene

Chemical Property:

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Technology Process of 1-(((2S,3S)-2-(benzyloxy)-5-methylhex-5-en-3-yloxy)methyl)-4-methoxybenzene

There total 4 articles about 1-(((2S,3S)-2-(benzyloxy)-5-methylhex-5-en-3-yloxy)methyl)-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 130323-28-3
(S,S)-2-methyl-5-(phenylmethoxy)hex-1-en-4-ol

: 824-94-2
p-methoxybenzyl chloride

: 1352481-37-8
1-(((2S,3S)-2-(benzyloxy)-5-methylhex-5-en-3-yloxy)methyl)-4-methoxybenzene

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol202966m

Reference yield:

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 1352481-37-8
1-(((2S,3S)-2-(benzyloxy)-5-methylhex-5-en-3-yloxy)methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: trifluorormethanesulfonic acid / Inert atmosphere

2: diisobutylaluminium hydride / Inert atmosphere

3: tin(IV) chloride / Inert atmosphere

4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C / Inert atmosphere

With trifluorormethanesulfonic acid; tin(IV) chloride; sodium hydride; diisobutylaluminium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol202966m

Reference yield:

: 54783-72-1
ethyl (S)-2-(benzyloxy)propionate

: 1352481-37-8
1-(((2S,3S)-2-(benzyloxy)-5-methylhex-5-en-3-yloxy)methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / Inert atmosphere

2: tin(IV) chloride / Inert atmosphere

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C / Inert atmosphere

With tin(IV) chloride; sodium hydride; diisobutylaluminium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol202966m