Technology Process of [3,3'-oxybis[((diphenylphosphino)methyl)benzen]ato(2-)-C2,C2',P,P'-d7]platinum(II)
There total 1 articles about [3,3'-oxybis[((diphenylphosphino)methyl)benzen]ato(2-)-C2,C2',P,P'-d7]platinum(II) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
neat (no solvent);
byproducts: HCl; Pt complex placed at bottom of Schlenk tube and covered with quartz wool plug, slow stream of N2 passed through tube, bottom of tube slowly heated to 250°C for 2 h and then to 270°C for 2 h; recrystd. from CH2Cl2-petroleum ether, elem. anal.;
DOI:10.1021/om00077a001