Technology Process of C43H49N9O13S2
There total 13 articles about C43H49N9O13S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(II) sulfate; sodium L-ascorbate;
In
water; dimethyl sulfoxide; tert-butyl alcohol;
at 20 - 25 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / methanol; water / 0.17 h / Reflux
2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C
3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C
4: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 3 h / 0 °C
5: potassium carbonate / methanol / 2 h / 20 °C
6: copper(II) sulfate; sodium L-ascorbate / dimethyl sulfoxide; tert-butyl alcohol / 20 °C
With
hydroxylamine hydrochloride; sodium acetate; sulfur trioxide pyridine complex; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; triethylamine; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1021/jm400560z
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / methanol; water / 0.17 h / Reflux
2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C
3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C
4: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 3 h / 0 °C
5: potassium carbonate / methanol / 2 h / 20 °C
6: copper(II) sulfate; sodium L-ascorbate / dimethyl sulfoxide; tert-butyl alcohol / 20 °C
With
hydroxylamine hydrochloride; sodium acetate; sulfur trioxide pyridine complex; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; triethylamine; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1021/jm400560z