(1S,2E)-benzoic acid 1-methyl-3-phenylallyl ester

Base Information

Chemical Name:(1S,2E)-benzoic acid 1-methyl-3-phenylallyl ester
CAS No.:135758-87-1
Molecular Formula:C₁₇H₁₆O₂
Molecular Weight:252.313
Hs Code.:

Synonyms:(1S,2E)-benzoic acid 1-methyl-3-phenylallyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2E)-benzoic acid 1-methyl-3-phenylallyl ester

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Technology Process of (1S,2E)-benzoic acid 1-methyl-3-phenylallyl ester

There total 4 articles about (1S,2E)-benzoic acid 1-methyl-3-phenylallyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 81176-43-4
(S)-trans-4-phenyl-3-buten-2-ol

: 98-88-4
benzoyl chloride

: 135758-87-1
(1S,2E)-benzoic acid 1-methyl-3-phenylallyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane;

Reference yield:

: 57194-69-1
cinnamaldehyde

: 135758-87-1
(1S,2E)-benzoic acid 1-methyl-3-phenylallyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) 4 A sieves, 2.) Et₃N, benzoyl chloride / 1.) hexane, lipase from Pseudomonas sp., 25 deg C, 12 h, 2.) CH₂Cl₂, 25 deg C, 15 h

With 4 A molecular sieve; benzoyl chloride; triethylamine;
DOI:10.1021/ja00016a032

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 36004-04-3
ethyl (E)-1-phenylbut-1-en-3-ol

: 84519-63-1
(R,E)-4-phenyl-3-buten-2-yl acetate

: 135758-87-1
(1S,2E)-benzoic acid 1-methyl-3-phenylallyl ester

Guidance literature:: With 4 A molecular sieve; benzoyl chloride; triethylamine; Yield given. Multistep reaction. Yields of byproduct given; 1.) hexane, lipase from Pseudomonas sp., 25 deg C, 12 h, 2.) CH₂Cl₂, 25 deg C, 15 h;
DOI:10.1021/ja00016a032