N-[2-(3-methoxyphenyl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)-2-oxoacetamide

Base Information

Chemical Name:N-[2-(3-methoxyphenyl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)-2-oxoacetamide
CAS No.:1447331-36-3
Molecular Formula:C₂₀H₂₁NO₇
Molecular Weight:387.389
Hs Code.:

Synonyms:N-[2-(3-methoxyphenyl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)-2-oxoacetamide

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Chemical Property of N-[2-(3-methoxyphenyl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)-2-oxoacetamide

Chemical Property:

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Technology Process of N-[2-(3-methoxyphenyl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)-2-oxoacetamide

There total 2 articles about N-[2-(3-methoxyphenyl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)-2-oxoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₉H₁₁NO₂*H⁽¹⁺⁾

: 88755-16-2
3,4,5-trimethoxybenzoylformic acid

: 1447331-36-3
N-[2-(3-methoxyphenyl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)-2-oxoacetamide

Guidance literature:: 3,4,5-trimethoxybenzoylformic acid; With 1,1'-carbonyldiimidazole; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 1h;

C₉H₁₁NO₂*H⁽¹⁺⁾; In 1-methyl-pyrrolidin-2-one; at 20 ℃;
DOI:10.1016/j.tetlet.2013.05.095

Reference yield:

: 1136-86-3
methyl (3,4,5-trimethoxyphenyl) ketone

: 1447331-36-3
N-[2-(3-methoxyphenyl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)-2-oxoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: selenium(IV) oxide; pyridine

2.1: 1,1'-carbonyldiimidazole / 1-methyl-pyrrolidin-2-one / 1 h / 20 °C

2.2: 20 °C

With pyridine; selenium(IV) oxide; 1,1'-carbonyldiimidazole; In 1-methyl-pyrrolidin-2-one;
DOI:10.1016/j.tetlet.2013.05.095

Reference yield: 60.0%

: 1447331-36-3
N-[2-(3-methoxyphenyl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)-2-oxoacetamide

: 1447330-86-0
5-(3-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)pyrazine-2(1H)-one

Guidance literature:: With ammonium acetate; In acetic acid; at 160 ℃; for 0.0666667h; Sealed tube; Microwave irradiation;
DOI:10.1016/j.tetlet.2013.05.095