C₂₄H₃₃NO₇

Base Information

Chemical Name:C₂₄H₃₃NO₇
CAS No.:1328886-20-9
Molecular Formula:C₂₄H₃₃NO₇
Molecular Weight:447.529
Hs Code.:

C<sub>24</sub>H<sub>33</sub>NO<sub>7</sub>

Synonyms:C₂₄H₃₃NO₇

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Chemical Property of C₂₄H₃₃NO₇

Chemical Property:

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Technology Process of C₂₄H₃₃NO₇

There total 5 articles about C₂₄H₃₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1328886-21-0
C₁₉H₂₅NO₅

: 108270-19-5
3-iodo-2-(methoxymethyloxy)-1-propene

: 1328886-20-9
C₂₄H₃₃NO₇

Guidance literature:: C₁₉H₂₅NO₅; With sodium hexamethyldisilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h;

3-iodo-2-(methoxymethyloxy)-1-propene; In tetrahydrofuran; toluene; at -78 - -45 ℃; diastereoselective reaction;
DOI:10.1055/s-0030-1260586

Reference yield:

: 2930-05-4,14618-80-5,89616-40-0,16495-13-9
(S)-benzyl glycidyl ether

: 1328886-20-9
C₂₄H₃₃NO₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / 1.17 h / 70 °C

1.2: 0.5 h / 20 °C

1.3: Heating

2.1: sodium hydride / tetrahydrofuran / 0 - 20 °C

2.2: 0 - 20 °C

3.1: triethylamine / diethyl ether / -78 - 0 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C

4.2: -78 - 0 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C

5.2: -78 - -45 °C

With n-butyllithium; sodium hexamethyldisilazane; sodium hydride; triethylamine; In tetrahydrofuran; diethyl ether; hexane; toluene;
DOI:10.1055/s-0030-1260586

Reference yield:

: C₁₈H₂₄O₅

: 1328886-20-9
C₂₄H₃₃NO₇

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C

1.2: -78 - 0 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C

2.2: -78 - -45 °C

With n-butyllithium; sodium hexamethyldisilazane; In tetrahydrofuran; hexane; toluene;
DOI:10.1055/s-0030-1260586