1-(2-methoxy-4-tributylstannylphenyl)-4-methyl-1H-imidazole

Base Information

• Chemical Name: 1-(2-methoxy-4-tributylstannylphenyl)-4-methyl-1H-imidazole
• CAS No.: 1160360-24-6
• Molecular Formula: C₂₃H₃₈N₂OSn
• Molecular Weight: 477.278
• Mol file: 1160360-24-6.mol

Synonyms:1-(2-methoxy-4-tributylstannylphenyl)-4-methyl-1H-imidazole

Chemical Property of 1-(2-methoxy-4-tributylstannylphenyl)-4-methyl-1H-imidazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2-methoxy-4-tributylstannylphenyl)-4-methyl-1H-imidazole

There total 1 articles about 1-(2-methoxy-4-tributylstannylphenyl)-4-methyl-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-bromo-2-methoxyphenyl)-4-methyl-1H-imidazole (870838-56-5) + bis(tri-n-butyltin) (813-19-4) → 1-(2-methoxy-4-tributylstannylphenyl)-4-methyl-1H-imidazole (1160360-24-6)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 120 ℃; for 2h;

Reference yield: 42.0%

1-(2-methoxy-4-tributylstannylphenyl)-4-methyl-1H-imidazole (1160360-24-6) + 4-bromo-1-(4-fluorobenzyl)indoline-2.3-dione (1021048-54-3) → C26H20FN3O3 (1160358-58-6)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 120 ℃; for 2h;

Reference yield: 11.0%

1-(2-methoxy-4-tributylstannylphenyl)-4-methyl-1H-imidazole (1160360-24-6) + C15H10BrF3N2 (1160359-93-2) → C26H21F3N4O (1160358-49-5)

Guidance literature:

1-(2-methoxy-4-tributylstannylphenyl)-4-methyl-1H-imidazole; C₁₅H₁₀BrF₃N₂; With caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; toluene; at 120 ℃;

With ammonium chloride; In water; N,N-dimethyl-formamide; toluene;

upstream raw materials:

1-(4-bromo-2-methoxyphenyl)-4-methyl-1H-imidazole

bis(tri-n-butyltin)

Downstream raw materials:

C₂₄H₂₀F₂N₆O₂

C₂₆H₂₀FN₃O₃

C₂₆H₂₄FN₃O

C₂₅H₂₁FN₄O