carboxybenzil α-octadecylaminobenzylphosphonic acid monoester

Base Information

Chemical Name:carboxybenzil α-octadecylaminobenzylphosphonic acid monoester
CAS No.:260396-74-5
Molecular Formula:C₃₉H₅₆NO₅P
Molecular Weight:649.851
Hs Code.:

Synonyms:carboxybenzil α-octadecylaminobenzylphosphonic acid monoester

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Chemical Property of carboxybenzil α-octadecylaminobenzylphosphonic acid monoester

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Technology Process of carboxybenzil α-octadecylaminobenzylphosphonic acid monoester

There total 5 articles about carboxybenzil α-octadecylaminobenzylphosphonic acid monoester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 261965-80-4,260396-65-4
5-(octadecylamino-phenyl-methyl)-3,3,8,8-tetraphenyl-1,4,6,9-tetraoxa-5λ⁵-phospha-spiro[4.4]nonane-2,7-dione

: 260396-74-5
carboxybenzil α-octadecylaminobenzylphosphonic acid monoester

Guidance literature:: With water; In acetonitrile; at 20 ℃;
DOI:10.1002/(SICI)1099-0690(200001)2000:2<281::AID-EJOC281>3.0.CO;2-2

Reference yield:

: 67422-90-6
3,3,8,8-tetraphenyl-1,4,6,9-tetraoxa-5λ⁵-phospha-spiro[4.4]nonane-2,7-dione

: 260396-74-5
carboxybenzil α-octadecylaminobenzylphosphonic acid monoester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CH₂Cl₂ / 20 °C

2: 78 percent / H₂O / acetonitrile / 20 °C

With water; In dichloromethane; acetonitrile; 1: Addition / 2: Hydrolysis;
DOI:10.1002/(SICI)1099-0690(200001)2000:2<281::AID-EJOC281>3.0.CO;2-2

Reference yield:

: 100-52-7
benzaldehyde

: 260396-74-5
carboxybenzil α-octadecylaminobenzylphosphonic acid monoester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / 3 Angstroem molecular sieves / CH₂Cl₂ / 6 h / 40 °C

2: 100 percent / CH₂Cl₂ / 20 °C

3: 78 percent / H₂O / acetonitrile / 20 °C

With 3 A molecular sieve; water; In dichloromethane; acetonitrile; 1: Condensation / 2: Addition / 3: Hydrolysis;
DOI:10.1002/(SICI)1099-0690(200001)2000:2<281::AID-EJOC281>3.0.CO;2-2