trans-1,1-dichloro-2,3-diethyl-2,3-bis(3-methoxyphenyl)-cyclopropane

Base Information

• Chemical Name: trans-1,1-dichloro-2,3-diethyl-2,3-bis(3-methoxyphenyl)-cyclopropane
• CAS No.: 84608-99-1
• Molecular Formula: C₂₁H₂₄Cl₂O₂
• Molecular Weight: 379.326
• Mol file: 84608-99-1.mol

Synonyms:trans-1,1-dichloro-2,3-diethyl-2,3-bis(3-methoxyphenyl)-cyclopropane

Chemical Property of trans-1,1-dichloro-2,3-diethyl-2,3-bis(3-methoxyphenyl)-cyclopropane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-1,1-dichloro-2,3-diethyl-2,3-bis(3-methoxyphenyl)-cyclopropane

There total 1 articles about trans-1,1-dichloro-2,3-diethyl-2,3-bis(3-methoxyphenyl)-cyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

chloroform (67-66-3,8013-54-5) + trans-3,3'-dimethoxy-α,β-diethylstilbene (76473-06-8) → trans-1,1-dichloro-2,3-diethyl-2,3-bis(3-methoxyphenyl)-cyclopropane (84608-99-1)

Guidance literature:

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; for 48h;

Reference yield: 48.0%

trans-1,1-dichloro-2,3-diethyl-2,3-bis(3-methoxyphenyl)-cyclopropane (84608-99-1) → trans-1,2-diethyl-1,2-bis-(3-methoxyphenyl)cyclopropane (84609-00-7)

Guidance literature:

With methanol; water; sodium; In diethyl ether; for 4h;

Reference yield:

trans-1,1-dichloro-2,3-diethyl-2,3-bis(3-methoxyphenyl)-cyclopropane (84608-99-1) → trans-<3,3'-(1,2-diethyl-1,2-cyclopropanediyl) bis (phenyl)>-diacetate (84609-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 48 percent / sodium, methanol, water / diethyl ether / 4 h

2: 1) BBr₃ 2) pyridine / 1) CH₂Cl₂, room t., 3 h; 2) reflux, 1 h

With pyridine; methanol; water; sodium; boron tribromide; In diethyl ether;

upstream raw materials:

chloroform

trans-3,3'-dimethoxy-α,β-diethylstilbene

Downstream raw materials:

trans-<3,3'-(3,3-dichloro-1,2-diethyl-1,2-cyclopropanediyl) bis (phenyl)>-diacetate

trans-1,2-diethyl-1,2-bis-(3-methoxyphenyl)cyclopropane

trans-<3,3'-(1,2-diethyl-1,2-cyclopropanediyl) bis (phenyl)>-diacetate