methyl (1-adamantyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate

Base Information

Chemical Name:methyl (1-adamantyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate
CAS No.:956107-32-7
Molecular Formula:C₂₉H₃₉NO₁₂S
Molecular Weight:625.694
Hs Code.:

Synonyms:methyl (1-adamantyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate

Suppliers and Price of methyl (1-adamantyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Arctom
Methyl(1-Adamantanyl5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-alpha-D-galacto-non-2-ulopyranoside)onate
250mg
$ 1980.00

Total 12 raw suppliers

Chemical Property of methyl (1-adamantyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Methyl(1-Adamantanyl5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-alpha-D-galacto-non-2-ulopyranoside)onate ^*data from reagent suppliers

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Useful:

Technology Process of methyl (1-adamantyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate

There total 3 articles about methyl (1-adamantyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl (7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-2-thioadamantyl-3,5-dideoxy-D-glycero-β-D-galactonon-2-ulopyranoside)onate

: 75-36-5
acetyl chloride

: 956107-32-7
methyl (1-adamantyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo7012912

Reference yield:

: C₂₀H₃₃NO₇S*ClH

: 956107-32-7
methyl (1-adamantyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / acetonitrile; water / 3 h / 20 °C / Inert atmosphere

2: pyridine / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / Inert atmosphere

With pyridine; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In water; acetonitrile;
DOI:10.1021/ja410683y

Reference yield:

: methyl (1-adamantyl 5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate

: 956107-32-7
methyl (1-adamantyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ylopyranosid)onate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / Inert atmosphere

With pyridine; N-ethyl-N,N-diisopropylamine;
DOI:10.1021/ja410683y