2-{2-{-2{-2(benzyloxy)propanoyloxy}propanoyloxy}propanoyloxy}propanoicacid-tert.butylester

Base Information

Chemical Name:2-{2-{-2{-2(benzyloxy)propanoyloxy}propanoyloxy}propanoyloxy}propanoicacid-tert.butylester
CAS No.:1053719-17-7
Molecular Formula:C₂₃H₃₂O₉
Molecular Weight:452.502
Hs Code.:

Synonyms:2-{2-{-2{-2(benzyloxy)propanoyloxy}propanoyloxy}propanoyloxy}propanoicacid-tert.butylester

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Chemical Property of 2-{2-{-2{-2(benzyloxy)propanoyloxy}propanoyloxy}propanoyloxy}propanoicacid-tert.butylester

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Technology Process of 2-{2-{-2{-2(benzyloxy)propanoyloxy}propanoyloxy}propanoyloxy}propanoicacid-tert.butylester

There total 3 articles about 2-{2-{-2{-2(benzyloxy)propanoyloxy}propanoyloxy}propanoyloxy}propanoicacid-tert.butylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 591244-66-5
2-{2-hydroxypropanoyloxy}propanoic acid tert-butyl ester

: 862999-87-9
2-{2-(benzyloxy)-propanoyloxy}propanoic acid

: 1053719-17-7
2-{2-{-2{-2(benzyloxy)propanoyloxy}propanoyloxy}propanoyloxy}propanoicacid-tert.butylester

Guidance literature:: 2-{2-(benzyloxy)-propanoyloxy}propanoic acid; With 2-chloro-1-methyl-pyridinium iodide; triethylamine; In dichloromethane; for 1h; Inert atmosphere; Reflux;

2-{2-hydroxypropanoyloxy}propanoic acid tert-butyl ester; In dichloromethane; for 20h; Inert atmosphere; Reflux;
DOI:10.1691/ph.2013.2686

Reference yield:

: 2-{2-(benzyloxy)-propanoyloxy}propanoic acid tert-butyl ester

: 1053719-17-7
2-{2-{-2{-2(benzyloxy)propanoyloxy}propanoyloxy}propanoyloxy}propanoicacid-tert.butylester

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 4 h / Reflux

2.1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 1 h / Inert atmosphere; Reflux

2.2: 20 h / Inert atmosphere; Reflux

With 2-chloro-1-methyl-pyridinium iodide; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1691/ph.2013.2686

Reference yield:

: 13650-70-9
(+)-tert-butyl D-lactate

: 1053719-17-7
2-{2-{-2{-2(benzyloxy)propanoyloxy}propanoyloxy}propanoyloxy}propanoicacid-tert.butylester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 48 h / Reflux

2.1: palladium 10% on activated carbon; hydrogen / diethyl ether

3.1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 1 h / Inert atmosphere; Reflux

3.2: 20 h / Inert atmosphere; Reflux

With palladium 10% on activated carbon; 2-chloro-1-methyl-pyridinium iodide; hydrogen; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1691/ph.2013.2686