piperidinium salt of 4,6-diphenyl-3-cyano-1,4-dihydropyridine-2-thiol

Base Information

Chemical Name:piperidinium salt of 4,6-diphenyl-3-cyano-1,4-dihydropyridine-2-thiol
CAS No.:148859-87-4
Molecular Formula:C₅H₁₁N*C₁₈H₁₄N₂S
Molecular Weight:375.538
Hs Code.:

Synonyms:piperidinium salt of 4,6-diphenyl-3-cyano-1,4-dihydropyridine-2-thiol

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Chemical Property of piperidinium salt of 4,6-diphenyl-3-cyano-1,4-dihydropyridine-2-thiol

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Technology Process of piperidinium salt of 4,6-diphenyl-3-cyano-1,4-dihydropyridine-2-thiol

There total 3 articles about piperidinium salt of 4,6-diphenyl-3-cyano-1,4-dihydropyridine-2-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7357-70-2
Cyanothioacetamide

: 82389-33-1
1-(2'-hydroxyethylthio)-1-phenyl-2-benzoyl-ethane

: 148859-87-4
piperidinium salt of 4,6-diphenyl-3-cyano-1,4-dihydropyridine-2-thiol

: 6-Hydroxy-2-mercapto-4,6-diphenyl-1,4,5,6-tetrahydro-pyridine-3-carbonitrile; compound with piperidine

Guidance literature:: With piperidine; In ethanol; Title compound not separated from byproducts; Ambient temperature;
DOI:10.1007/BF00479355

Reference yield:

: 110-89-4
piperidine

: 7357-70-2
Cyanothioacetamide

: 614-47-1
1,3-diphenyl-propen-3-one

: 148859-87-4
piperidinium salt of 4,6-diphenyl-3-cyano-1,4-dihydropyridine-2-thiol

Guidance literature:: In ethanol; at 0 ℃; for 1h;
DOI:10.1081/SCC-120021503

Reference yield:

: 94-41-7
benzalacetophenone

: 148859-87-4
piperidinium salt of 4,6-diphenyl-3-cyano-1,4-dihydropyridine-2-thiol

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / KOH / ethanol / Heating

2: piperidine / ethanol / Ambient temperature

With piperidine; potassium hydroxide; In ethanol;
DOI:10.1007/BF00479355