Methyl 2-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]acetate

Base Information

• Chemical Name: Methyl 2-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]acetate
• CAS No.: 227304-75-8
• Molecular Formula: C₂₁H₂₃NO₄S
• Molecular Weight: 385.484

Synonyms:Methyl 2-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]acetate

Chemical Property of Methyl 2-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]acetate

Chemical Property:

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Technology Process of Methyl 2-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]acetate

There total 3 articles about Methyl 2-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4(3-Methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridine (227304-73-6) + chlorosulfonyl-acetic acid methyl ester (56146-83-9) → Methyl 2-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]acetate (227304-75-8)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.bmcl.2007.10.042

Reference yield:

→ Methyl 2-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]acetate (227304-75-8)

Guidance literature:

Reference yield:

→ Methyl 2-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]acetate (227304-75-8) + Methyl 4-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]tetrahydropyran-4-carboxylate (227305-86-4)

Guidance literature:

upstream raw materials:

4(3-Methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridine

chlorosulfonyl-acetic acid methyl ester

Downstream raw materials:

N-Hydroxy-2-[4-(3-methyl-4-phenylphenyl)-1,2,3,6-tetrahydropyridin-1-ylsulphonyl]acetamide

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