methyl (E)-4,5-dihydroxy-2-methoxy-β-methylcinnamate

Base Information

Chemical Name:methyl (E)-4,5-dihydroxy-2-methoxy-β-methylcinnamate
CAS No.:172798-42-4
Molecular Formula:C₁₂H₁₄O₅
Molecular Weight:238.24
Hs Code.:

Synonyms:methyl (E)-4,5-dihydroxy-2-methoxy-β-methylcinnamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (E)-4,5-dihydroxy-2-methoxy-β-methylcinnamate

Chemical Property:

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Technology Process of methyl (E)-4,5-dihydroxy-2-methoxy-β-methylcinnamate

There total 8 articles about methyl (E)-4,5-dihydroxy-2-methoxy-β-methylcinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6345-62-6
6-hydroxy-7-methoxyl-4-methylcoumarin

: methyl (Z)-4,5-dihydroxy-2-methoxy-β-methylcinnamate

: 172798-42-4
methyl (E)-4,5-dihydroxy-2-methoxy-β-methylcinnamate

Guidance literature:: Multi-step reaction with 3 steps

1: [bis(acetoxy)iodo]benzene; toluene-4-sulfonic acid / 1 h / 20 °C

2: sodium dithionite / water / 1 h / 20 °C

3: sulfuric acid / 84 h / 20 °C

With sodium dithionite; [bis(acetoxy)iodo]benzene; sulfuric acid; toluene-4-sulfonic acid; In water;
DOI:10.1002/ejoc.201901894

Reference yield:

: 824-46-4
methoxyhydroquinone

: methyl (Z)-4,5-dihydroxy-2-methoxy-β-methylcinnamate

: 172798-42-4
methyl (E)-4,5-dihydroxy-2-methoxy-β-methylcinnamate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / water / 18 h / 20 °C

2: [bis(acetoxy)iodo]benzene; toluene-4-sulfonic acid / 1 h / 20 °C

3: sodium dithionite / water / 1 h / 20 °C

4: sulfuric acid / 84 h / 20 °C

With sodium dithionite; [bis(acetoxy)iodo]benzene; sulfuric acid; toluene-4-sulfonic acid; In water;
DOI:10.1002/ejoc.201901894

Reference yield:

: 121-33-5,8014-42-4
vanillin

: methyl (Z)-4,5-dihydroxy-2-methoxy-β-methylcinnamate

: 172798-42-4
methyl (E)-4,5-dihydroxy-2-methoxy-β-methylcinnamate

Guidance literature:: Multi-step reaction with 5 steps

1: dihydrogen peroxide; potassium hydroxide / water / 0.67 h / 40 °C

2: sulfuric acid / water / 18 h / 20 °C

3: [bis(acetoxy)iodo]benzene; toluene-4-sulfonic acid / 1 h / 20 °C

4: sodium dithionite / water / 1 h / 20 °C

5: sulfuric acid / 84 h / 20 °C

With sodium dithionite; [bis(acetoxy)iodo]benzene; sulfuric acid; dihydrogen peroxide; toluene-4-sulfonic acid; potassium hydroxide; In water;
DOI:10.1002/ejoc.201901894