Fmoc-Leu-OKb, Kb=2,4-didocosyloxybenzyl

Base Information

Chemical Name:Fmoc-Leu-OKb, Kb=2,4-didocosyloxybenzyl
CAS No.:1399051-25-2
Molecular Formula:C₇₂H₁₁₇NO₆
Molecular Weight:1092.72
Hs Code.:

Synonyms:Fmoc-Leu-OKb, Kb=2,4-didocosyloxybenzyl

Suppliers and Price of Fmoc-Leu-OKb, Kb=2,4-didocosyloxybenzyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Fmoc-Leu-OKb, Kb=2,4-didocosyloxybenzyl

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Fmoc-Leu-OKb, Kb=2,4-didocosyloxybenzyl

There total 4 articles about Fmoc-Leu-OKb, Kb=2,4-didocosyloxybenzyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

: 931120-51-3
2,4-bis(docosyloxy)benzyl alcohol

: 35661-60-0
Fmoc-Leu-OH

: 1399051-25-2
Fmoc-Leu-OKb, Kb=2,4-didocosyloxybenzyl

Guidance literature:: With dmap; diisopropyl-carbodiimide; In dichloromethane;

Reference yield:

: 931120-54-6
Kb-Gly-H

: 1399051-25-2
Fmoc-Leu-OKb, Kb=2,4-didocosyloxybenzyl

Guidance literature:: Multi-step reaction with 3 steps

1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

2: Montmorillonite K₁₀ / dichloromethane / 3.5 h / 20 °C

3: diisopropyl-carbodiimide; dmap / N,N-dimethyl-formamide / 1 h / 55 °C

With dmap; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 931120-53-5
Fmoc-Gly-OKb, Kb=2,4-didocosyloxybenzyl

: 1399051-25-2
Fmoc-Leu-OKb, Kb=2,4-didocosyloxybenzyl

Guidance literature:: Multi-step reaction with 4 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / 20 °C

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

3: Montmorillonite K₁₀ / dichloromethane / 3.5 h / 20 °C

4: diisopropyl-carbodiimide; dmap / N,N-dimethyl-formamide / 1 h / 55 °C

With dmap; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;