N-(3,5-dimethoxyphenyl)-4-nitrobenzamide

Base Information

Chemical Name:N-(3,5-dimethoxyphenyl)-4-nitrobenzamide
CAS No.:152586-91-9
Molecular Formula:C₁₅H₁₄N₂O₅
Molecular Weight:302.287
Hs Code.:
DSSTox Substance ID:DTXSID501274716

Synonyms:N-(3,5-dimethoxyphenyl)-4-nitrobenzamide;152586-91-9;Cambridge id 5107183;Oprea1_516590;CBDivE_000558;SCHEMBL4248472;DTXSID501274716;MFCD00406461;AKOS008558114;AB00073793-01

Suppliers and Price of N-(3,5-dimethoxyphenyl)-4-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(3,5-dimethoxyphenyl)-4-nitrobenzamide

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:302.09027155
Heavy Atom Count:22
Complexity:378

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC(=CC(=C1)NC(=O)C2=CC=C(C=C2)[N+](=O)[O-])OC

Technology Process of N-(3,5-dimethoxyphenyl)-4-nitrobenzamide

There total 1 articles about N-(3,5-dimethoxyphenyl)-4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 122-04-3
4-nitro-benzoyl chloride

: 10272-07-8
3.5-dimethoxyaniline

: 152586-91-9
N-(3,5-dimethoxyphenyl)-4-nitrobenzamide

Guidance literature:: With pyridine; for 2h; Heating;
DOI:10.1021/jm9600959

Reference yield: 90.0%

: 152586-91-9
N-(3,5-dimethoxyphenyl)-4-nitrobenzamide

: 178803-99-1
N-(3,5-dimethoxyphenyl)-4-nitrobenzothioamide

Guidance literature:: With Lawessons reagent; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 100 ℃; for 6h;
DOI:10.1021/jm9600959

Reference yield:

: 152586-91-9
N-(3,5-dimethoxyphenyl)-4-nitrobenzamide

: 178804-14-3
4-(5,7-dimethoxybenzo[d]thiazol-2-yl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 2,4-bis(4-methoxyphenyl)-2,4-dithioxo-1,3,2,4-dithiadiphosphetane / hexamethylphosphoric acid triamide / 6 h / 100 °C

2: 60 percent / 10percent aq. NaOH, potassium ferricyanide / ethanol / 0.5 h / 80 - 90 °C

3: 90 percent / SnCl₂*2H₂O / ethanol / 4 h / Heating

With Lawessons reagent; sodium hydroxide; tin(ll) chloride; potassium hexacyanoferrate(III); In N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol;
DOI:10.1021/jm9600959