[((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)Ti(CH₂(t-Bu))2

Base Information

Chemical Name:[((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)Ti(CH₂(t-Bu))2
CAS No.:851530-58-0
Molecular Formula:C₄₅H₇₅N₂Ti
Molecular Weight:691.984
Hs Code.:

[((C<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2-2,6)Ti(CH<sub>2</sub>(t-Bu))2

Synonyms:[((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)Ti(CH₂(t-Bu))2

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Chemical Property of [((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)Ti(CH₂(t-Bu))2

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Technology Process of [((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)Ti(CH₂(t-Bu))2

There total 2 articles about [((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)Ti(CH₂(t-Bu))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 851530-56-8
(^tBunacnac)TiCl₂

: 7412-67-1
neopentyl lithium

: 851530-58-0
[((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)Ti(CH₂(t-Bu))2

Guidance literature:: In diethyl ether; N2 atm.; to a cold soln. (-35°C) of complex in diethyl ether was added a cold diethyl ether-soln. of Li-compound, stirred for 30 min; filtered, dried under reduced pressure, extd. with hexane, filtered, concd., cooled to -35°C;
DOI:10.1021/om049400b

Reference yield:

: Li[((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)]

: 851530-58-0
[((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)Ti(CH₂(t-Bu))2

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: diethyl ether

In diethyl ether; toluene;
DOI:10.1021/om049400b

Reference yield: 83.0%

: 851530-58-0
[((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)Ti(CH₂(t-Bu))2

: 2923-28-6
silver trifluoromethanesulfonate

: [((C₆H₃(CH(CH₃)2)2-2,6)NC(t-Bu)CHC(t-Bu)N(C₆H₃(CH(CH₃)2)2-2,6)Ti(=CH(t-Bu))(OTf)

Guidance literature:: In tetrahydrofuran; N2 atm.; to a cold (-35°C) soln. of complex in THF was added a cold THF-soln.of AgOSO2CF3, stirred for 20 min; filtered, dried under reduced pressure, extd. with hexane, filtered, concd., cooled to -35°C; elem. anal.;
DOI:10.1021/om049400b