2-<<(Benzyloxy)methoxy>methyl>-3-<(tert-butyldimethylsilyl)oxy>-1-propanol

Base Information

• Chemical Name: 2-<<(Benzyloxy)methoxy>methyl>-3-<(tert-butyldimethylsilyl)oxy>-1-propanol
• CAS No.: 950902-11-1
• Molecular Formula: C₁₈H₃₂O₄Si
• Molecular Weight: 340.535

Synonyms:2-<<(Benzyloxy)methoxy>methyl>-3-<(tert-butyldimethylsilyl)oxy>-1-propanol

Chemical Property of 2-<<(Benzyloxy)methoxy>methyl>-3-<(tert-butyldimethylsilyl)oxy>-1-propanol

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Technology Process of 2-<<(Benzyloxy)methoxy>methyl>-3-<(tert-butyldimethylsilyl)oxy>-1-propanol

There total 14 articles about 2-<<(Benzyloxy)methoxy>methyl>-3-<(tert-butyldimethylsilyl)oxy>-1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

ethyl 2-{[(benzyloxy)methoxy]methyl}-3-[(tert-butyl)dimethylsilyloxy]propanoate (950902-09-7) → 2-<<(Benzyloxy)methoxy>methyl>-3-<(tert-butyldimethylsilyl)oxy>-1-propanol (950902-11-1)

Guidance literature:

With lithium borohydride; In tetrahydrofuran; ethanol; at 20 - 40 ℃; for 19h;

DOI:10.1002/hlca.200790144

Reference yield: 92.0%

(R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde (133377-92-1) → 2-<<(Benzyloxy)methoxy>methyl>-3-<(tert-butyldimethylsilyl)oxy>-1-propanol (950902-11-1)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 0.25h; Ambient temperature;

DOI:10.1021/jo00031a039

Reference yield: 92.0%

(S)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde (135218-62-1) → 2-<<(Benzyloxy)methoxy>methyl>-3-<(tert-butyldimethylsilyl)oxy>-1-propanol (950902-11-1)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 0.25h; Ambient temperature;

DOI:10.1021/jo00031a039

upstream raw materials:

(R)-3-(tert-Butyl-dimethyl-silanyloxy)-2-cyclohexylidenemethyl-propan-1-ol

(R)-(E)-2-<<(Benzyloxy)methoxy>methyl>-1-<<(tert-butyldimethylsilyl)oxy>methyl>non-3-en

(R)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde

(S)-2-Benzyloxymethoxymethyl-3-(tert-butyl-dimethyl-silanyloxy)-propionaldehyde

Downstream raw materials:

2-{[(benzyloxy)methoxy]methyl}-3-[(tert-butyl)dimethylsilyloxy]propyl methanesulfonate

2-(2-{[(benzyloxy)methoxy]methyl}-3-[(tert-butyl)dimethylsilyloxy]propylamino)-1-phenylethanol

tert-butyl N-(2-hydroxy-2-phenylethyl)-N-(2-{[(benzyloxy)methoxy]methyl}-3-[(tert-butyl)dimethylsilyloxy]propyl)carbamate

tert-butyl N-(2-{[(benzyloxy)methoxy]methyl}-3-[(tert-butyl)dimethylsilyloxy]propyl)-N-(2-oxo-2-phenylethyl)carbamate

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