Methyl 3-(2-Methoxy-5-methylphenyl)-1,5-dimethoxy-4-(benzyloxy)-2-naphthoate

Base Information

• Chemical Name: Methyl 3-(2-Methoxy-5-methylphenyl)-1,5-dimethoxy-4-(benzyloxy)-2-naphthoate
• CAS No.: 74724-87-1
• Molecular Formula: C₂₉H₂₈O₆
• Molecular Weight: 472.538

Synonyms:Methyl 3-(2-Methoxy-5-methylphenyl)-1,5-dimethoxy-4-(benzyloxy)-2-naphthoate

Chemical Property of Methyl 3-(2-Methoxy-5-methylphenyl)-1,5-dimethoxy-4-(benzyloxy)-2-naphthoate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of Methyl 3-(2-Methoxy-5-methylphenyl)-1,5-dimethoxy-4-(benzyloxy)-2-naphthoate

There total 4 articles about Methyl 3-(2-Methoxy-5-methylphenyl)-1,5-dimethoxy-4-(benzyloxy)-2-naphthoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) → Methyl 3-(2-Methoxy-5-methylphenyl)-1,5-dimethoxy-4-(benzyloxy)-2-naphthoate (74724-87-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 56 percent / K₂CO₃ / acetone / Heating

2: 1.) K₂CO₃, 2.) triethylamine / 1.) acetone, reflux, overnight; 2.) ether, 1h

With potassium carbonate; triethylamine; In acetone;

DOI:10.1021/jo01309a001

Reference yield:

7,12-dihydroxy-11-methoxy-2-methyl-6H-benzo-naphtho<2,3-d>pyran-6-one (74724-84-8) → Methyl 3-(2-Methoxy-5-methylphenyl)-1,5-dimethoxy-4-(benzyloxy)-2-naphthoate (74724-87-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 56 percent / K₂CO₃ / acetone / Heating

2: 1.) K₂CO₃, 2.) triethylamine / 1.) acetone, reflux, overnight; 2.) ether, 1h

With potassium carbonate; triethylamine; In acetone;

DOI:10.1021/jo01309a001

Reference yield:

2-Methyl-7-hydroxy-11-methoxy-12-(benzyloxy)-6H-benzonaphtho<2,3-d>pyran-6-one (74724-85-9) → Methyl 3-(2-Methoxy-5-methylphenyl)-1,5-dimethoxy-4-(benzyloxy)-2-naphthoate (74724-87-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) K₂CO₃, 2.) triethylamine / 1.) acetone, reflux, overnight; 2.) ether, 1h

With potassium carbonate; triethylamine;

DOI:10.1021/jo01309a001

upstream raw materials:

2-Methyl-7,11-dimethoxy-12-(benzyloxy)-6H-benzo-naphtho<2,3-d>pyran-6-one

dimethyl sulfate

benzyl bromide

7,12-dihydroxy-11-methoxy-2-methyl-6H-benzo-naphtho<2,3-d>pyran-6-one

Downstream raw materials:

Methyl 3-(2-Methoxy-5-methylphenyl)-1,5-dimethoxy-4-hydroxy-2-naphthoate

chartarin

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